tert-butyl-[7-(3,6-diisopropoxy-2-methoxyphenyl)heptyloxy]dimethylsilane

Base Information

Chemical Name:tert-butyl-[7-(3,6-diisopropoxy-2-methoxyphenyl)heptyloxy]dimethylsilane
CAS No.:865838-59-1
Molecular Formula:C₂₆H₄₈O₄Si
Molecular Weight:452.75
Hs Code.:

Synonyms:tert-butyl-[7-(3,6-diisopropoxy-2-methoxyphenyl)heptyloxy]dimethylsilane

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Chemical Property of tert-butyl-[7-(3,6-diisopropoxy-2-methoxyphenyl)heptyloxy]dimethylsilane

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Technology Process of tert-butyl-[7-(3,6-diisopropoxy-2-methoxyphenyl)heptyloxy]dimethylsilane

There total 1 articles about tert-butyl-[7-(3,6-diisopropoxy-2-methoxyphenyl)heptyloxy]dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 78535-68-9
7-[(tert-butyl)dimethylsilyloxy]-1-iodoheptane

: 96501-81-4
1,4-diisopropyloxy-2-methoxybenzene

: 865838-59-1
tert-butyl-[7-(3,6-diisopropoxy-2-methoxyphenyl)heptyloxy]dimethylsilane

Guidance literature:: 1,4-diisopropyloxy-2-methoxybenzene; With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃;

7-[(tert-butyl)dimethylsilyloxy]-1-iodoheptane; In tetrahydrofuran; hexane; at 20 ℃; for 14h;
DOI:10.1055/s-2005-869970

Reference yield: 90.0%

: 865838-59-1
tert-butyl-[7-(3,6-diisopropoxy-2-methoxyphenyl)heptyloxy]dimethylsilane

: 865838-60-4
7-(3,6-diisopropoxy-2-methoxyphenyl)heptan-1-ol

Guidance literature:: With acetic acid; In tetrahydrofuran; at 20 ℃;
DOI:10.1055/s-2005-869970

Reference yield:

: 865838-59-1
tert-butyl-[7-(3,6-diisopropoxy-2-methoxyphenyl)heptyloxy]dimethylsilane

: 865838-65-9
(2E)-9-(3,6-diisopropoxy-2-methoxyphenyl)-2-methylnon-2-enal

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / aq. AcOH / tetrahydrofuran / 20 °C

2: 89 percent / oxalyl chloride; Et₃N; DMSO / CH₂Cl₂ / -78 - 20 °C

3: 94 percent / toluene / 12 h / 60 °C

4: 90 percent / LiAlH₄ / diethyl ether / 2 h / 20 °C

5: 91 percent / oxalyl chloride; Et₃N; DMSO / CH₂Cl₂ / -78 - 20 °C

With lithium aluminium tetrahydride; oxalyl dichloride; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; 2: Swern oxidation / 3: Witting reaction / 5: Swern oxidation;
DOI:10.1055/s-2005-869970