Diethyldithiocarbamic Acid Copper Salt

Base Information

• Chemical Name: Diethyldithiocarbamic Acid Copper Salt
• CAS No.: 13681-87-3
• Molecular Formula: C10H20 Cu N2 S4
• Molecular Weight: 360.092
• Hs Code.: 2930909090
• Mol file: 13681-87-3.mol

Synonyms:bis(N,N-diethyldithiocarbamate)Cu (II) complex;Cu-DDC complex

Chemical Property of Diethyldithiocarbamic Acid Copper Salt

Chemical Property:

• Melting Point: 197°C
• Boiling Point: 176.4°Cat760mmHg
• Flash Point: 60.5°C
• PSA: 134.68000
• Density: g/cm³
• LogP: 3.08330
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 358.980530
• Heavy Atom Count: 17
• Complexity: 185

Purity/Quality:

99% ^*data from raw suppliers

Copper(II) Diethyldithiocarbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Moderately toxic by ingestion.
• Hazard Codes: Moderately toxic by ingestion.
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)C(=S)[S-].CCN(CC)C(=S)[S-].[Cu+2]
• Uses: Agricultural chemical.

Technology Process of Diethyldithiocarbamic Acid Copper Salt

There total 21 articles about Diethyldithiocarbamic Acid Copper Salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

sodium N,N-diethyldithiocarbamate (148-18-5) + copper dichloride → bis(N,N-diethyldithiocarbamato)copper(II) (13681-87-3)

Guidance literature:

In neat (no solvent, solid phase); byproducts: NaCl; placing of CuCl2 and NaS2CNEt2 in 1:2 ratio to the reactor; sealing, vibrating for 60 min; sublimating in vac. at 180-190°C; crystn.; elem. anal.;

DOI:10.1134/S0036023607060083

Reference yield: 96.0%

copper(II) chloride hexahydrate + sodium N,N-diethyldithiocarbamate (148-18-5) → copper(II) bis(diethyldithiocarbamate) (13681-87-3)

Guidance literature:

In water; at 20 ℃; for 1h;

DOI:10.1002/jccs.202000504

Reference yield: 95.0%

copper diacetate (142-71-2) + diethylamine (109-89-7) → bis(N,N-diethyldithiocarbamato)copper(II) (13681-87-3)

Guidance literature:

With carbon disulfide; In acetonitrile; diethylamine added to a soln. of per(II) acetate, then CS2 (6-fold excess) added dropwise with stirring, stirred (room temp., 1 h); solvent removed (reduced presure), ppt. dissolved (acetone), pptd. (water), filtered, washed (water), dried (60°C); elem. anal.; Kinetics;

upstream raw materials:

disulfiram

copper

carbon disulfide

diethylamine

Downstream raw materials:

bis(N,N-diethyldithiocarbamato)mercury(II)

copper(II) dithizonate (diethyl dithiocarbamate)

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