(2S,5R)-2,2,2-trichloroethyl 2-(hydroxymethyl)-5-phenylmorpholine-4-carboxylate

Base Information

Chemical Name:(2S,5R)-2,2,2-trichloroethyl 2-(hydroxymethyl)-5-phenylmorpholine-4-carboxylate
CAS No.:1349829-39-5
Molecular Formula:C₁₄H₁₆Cl₃NO₄
Molecular Weight:368.644
Hs Code.:

Synonyms:(2S,5R)-2,2,2-trichloroethyl 2-(hydroxymethyl)-5-phenylmorpholine-4-carboxylate

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Chemical Property of (2S,5R)-2,2,2-trichloroethyl 2-(hydroxymethyl)-5-phenylmorpholine-4-carboxylate

Chemical Property:

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Technology Process of (2S,5R)-2,2,2-trichloroethyl 2-(hydroxymethyl)-5-phenylmorpholine-4-carboxylate

There total 1 articles about (2S,5R)-2,2,2-trichloroethyl 2-(hydroxymethyl)-5-phenylmorpholine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.6%

: 1349829-37-3
((2S,5R)-5-phenylmorpholin-2-yl)methanol

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 1349829-39-5
(2S,5R)-2,2,2-trichloroethyl 2-(hydroxymethyl)-5-phenylmorpholine-4-carboxylate

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃;

Reference yield: 46.0%

: 1349829-39-5
(2S,5R)-2,2,2-trichloroethyl 2-(hydroxymethyl)-5-phenylmorpholine-4-carboxylate

: 202289-38-1
(bis-(2-methoxyethyl)amino)sulfur trufluoride

: 1349829-40-8
(2S,5R)-2,2,2-trichloroethyl 2-(fluoromethyl)-5-phenylmorpholine-4-carboxylate

Guidance literature:: (2S,5R)-2,2,2-trichloroethyl 2-(hydroxymethyl)-5-phenylmorpholine-4-carboxylate; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In 1,2-dichloro-ethane; toluene; at 0 - 20 ℃;

With sodium hydroxide; In dichloromethane; water;

Reference yield:

: 1349829-39-5
(2S,5R)-2,2,2-trichloroethyl 2-(hydroxymethyl)-5-phenylmorpholine-4-carboxylate

: 1349829-35-1
(2S,5R)-2-(fluoromethyl)-5-phenylmorpholine

Guidance literature:: Multi-step reaction with 2 steps

1: toluene; 1,2-dichloro-ethane / 0 - 20 °C

2: zinc; acetic acid / 60 °C

With acetic acid; zinc; In 1,2-dichloro-ethane; toluene;