N-cyanomethylhippuric acid

Base Information

Chemical Name:N-cyanomethylhippuric acid
CAS No.:152189-69-0
Molecular Formula:C₁₁H₁₀N₂O₃
Molecular Weight:218.212
Hs Code.:

Synonyms:N-cyanomethylhippuric acid

Suppliers and Price of N-cyanomethylhippuric acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cyanomethylhippuric acid

Chemical Property:

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Technology Process of N-cyanomethylhippuric acid

There total 1 articles about N-cyanomethylhippuric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: α-(cyanomethylamino)acetic acid

: 152189-69-0
N-cyanomethylhippuric acid

Guidance literature:: With sodium hydrogencarbonate; In water; at 20 ℃; for 1.5h; Yield given;
DOI:10.1007/BF00531659

Reference yield:

: 152189-69-0
N-cyanomethylhippuric acid

: 55375-91-2,57989-66-9,54761-87-4,55375-89-8
(-)-2-Benzoyl-4-oxo-1,2,3,6,7,11b-hexahydro-4H-pyrazino[2,1-a]isoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) dicyclohexylcarbodiimide / 1.) acetonitrile, 20 deg C, 30 min, 2.) acetonitrile, 20 deg C, 24 h

2: 45 percent / formic acid, Raney Ni / H₂O / 2 h / Heating

3: 83 percent / conc. H₂SO₄ / 3 h / 20 °C

With formic acid; sulfuric acid; nickel; dicyclohexyl-carbodiimide; In water;
DOI:10.1007/BF00531659

Reference yield:

: 152189-69-0
N-cyanomethylhippuric acid

: 87693-80-9
1-(2-phenylethyl)-4-benzoyl-2-hydroxypiperazin-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dicyclohexylcarbodiimide / 1.) acetonitrile, 20 deg C, 30 min, 2.) acetonitrile, 20 deg C, 24 h

2: 23 percent / formic acid, Raney Ni / H₂O / 2 h / Heating

With formic acid; nickel; dicyclohexyl-carbodiimide; In water;
DOI:10.1007/BF00531659