Technology Process of C57H56O12
There total 4 articles about C57H56O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H28O5;
With
sodium hydrogencarbonate;
In
dichloromethane;
at 25 ℃;
for 0.5h;
Inert atmosphere;
malonoyl dichloride;
In
dichloromethane;
at 25 ℃;
Inert atmosphere;
DOI:10.1039/b922740g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium tert-butylate / N,N-dimethyl-formamide / 4 h / 25 °C / Inert atmosphere
2.1: potassium tert-butylate / N,N-dimethyl-formamide / 3 h / 25 °C / Inert atmosphere
3.1: sodium hydrogencarbonate / dichloromethane / 0.5 h / 25 °C / Inert atmosphere
3.2: 25 °C / Inert atmosphere
With
potassium tert-butylate; sodium hydrogencarbonate;
In
dichloromethane; N,N-dimethyl-formamide;
1.1: Horner-Emmons-Wittig coupling / 2.1: Horner-Emmons-Wittig coupling;
DOI:10.1039/b922740g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium tert-butylate / N,N-dimethyl-formamide / 4 h / 25 °C / Inert atmosphere
2.1: potassium tert-butylate / N,N-dimethyl-formamide / 3 h / 25 °C / Inert atmosphere
3.1: sodium hydrogencarbonate / dichloromethane / 0.5 h / 25 °C / Inert atmosphere
3.2: 25 °C / Inert atmosphere
With
potassium tert-butylate; sodium hydrogencarbonate;
In
dichloromethane; N,N-dimethyl-formamide;
1.1: Horner-Emmons-Wittig coupling / 2.1: Horner-Emmons-Wittig coupling;
DOI:10.1039/b922740g
