ethyl 3-biphenyl-4-yl>methyl>amino>pyridine-4-carboxylate

Base Information

Chemical Name:ethyl 3-biphenyl-4-yl>methyl>amino>pyridine-4-carboxylate
CAS No.:151323-71-6
Molecular Formula:C₄₄H₄₀N₆O₂
Molecular Weight:684.841
Hs Code.:

ethyl 3-<N-propyl-N-<<2'-<2-(triphenylmethyl)-2H-tetrazol-5-yl>biphenyl-4-yl>methyl>amino>pyridine-4-carboxylate

Synonyms:ethyl 3-biphenyl-4-yl>methyl>amino>pyridine-4-carboxylate

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Chemical Property of ethyl 3-biphenyl-4-yl>methyl>amino>pyridine-4-carboxylate

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Technology Process of ethyl 3-biphenyl-4-yl>methyl>amino>pyridine-4-carboxylate

There total 3 articles about ethyl 3-biphenyl-4-yl>methyl>amino>pyridine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7579-20-6
3-Aminopyridine-4-carboxylic acid

: 151323-71-6
ethyl 3-biphenyl-4-yl>methyl>amino>pyridine-4-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂SO₄ / 4 h / Heating

2: 1.) DMPU, lithium hexamethyl disilazide / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, overnight

3: 448 mg / H₂ / PtO₂ / ethyl acetate

4: 1.) 1,3-dimethyl-3,4,5,6-tetrahydro-2-pyrimidinone, LiN(TMS)2 / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 90 min

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sulfuric acid; hydrogen; lithium hexamethyldisilazane; platinum(IV) oxide; In ethyl acetate;
DOI:10.1021/jm00070a012

Reference yield:

: 14208-83-4
ethyl 3-aminopyridine-4-carboxylate

: 151323-71-6
ethyl 3-biphenyl-4-yl>methyl>amino>pyridine-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) DMPU, lithium hexamethyl disilazide / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, overnight

2: 448 mg / H₂ / PtO₂ / ethyl acetate

3: 1.) 1,3-dimethyl-3,4,5,6-tetrahydro-2-pyrimidinone, LiN(TMS)2 / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 90 min

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; hydrogen; lithium hexamethyldisilazane; platinum(IV) oxide; In ethyl acetate;
DOI:10.1021/jm00070a012

Reference yield:

: 157361-40-5
ethyl 3-allylaminopyridine-4-carboxylate

: 151323-71-6
ethyl 3-biphenyl-4-yl>methyl>amino>pyridine-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 448 mg / H₂ / PtO₂ / ethyl acetate

2: 1.) 1,3-dimethyl-3,4,5,6-tetrahydro-2-pyrimidinone, LiN(TMS)2 / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 90 min

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; hydrogen; lithium hexamethyldisilazane; platinum(IV) oxide; In ethyl acetate;
DOI:10.1021/jm00070a012