(NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂

Base Information

Chemical Name:(NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂
CAS No.:583878-62-0
Molecular Formula:C₅₀H₁₁₄N₆Nb₂P₄Si₈
Molecular Weight:1333.89
Hs Code.:

(NbCH<sub>3</sub>(PC<sub>6</sub>H<sub>11</sub>)2(CH<sub>2</sub>Si(CH<sub>3</sub>)2)4N<sub>2</sub>)2N<sub>2</sub>

Synonyms:(NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂

Suppliers and Price of (NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂

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Chemical Property of (NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂

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Technology Process of (NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂

There total 2 articles about (NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 583878-58-4
NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂

: 7727-37-9
nitrogen

: 583878-62-0
(NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂

Guidance literature:: In toluene; soln. of complex in toluene was exposed to an atm. of N2, stirred for 6 h; solvent was removed in vac., extd. with toluene, filtered, the solvent was removed, solid was washed with hexane; elem. anal.;
DOI:10.1016/S0020-1693(02)01305-1

Reference yield:

: 583878-58-4
NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂

: 7727-37-9
nitrogen

: 676-58-4
methylmagnesium chloride

: 583878-62-0
(NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂

Guidance literature:: In toluene; byproducts: MgCl2; CH3MgCl was slowly added to a stirred soln. of complex in toluene under N2; solvent was removed in vac., extd. with toluene, filtered, the solvent was removed, solid was washed with hexane; elem. anal.;
DOI:10.1016/S0020-1693(02)01305-1

Reference yield: 82.0%

: 583878-62-0
(NbCH₃(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂

: 583878-66-4
(Nb(PC₆H₁₁)2(CH₂Si(CH₃)2)4N₂)2N₂

Guidance literature:: With H₂; In toluene; a soln. of complex in toluene was placed under 1 atm of H2, stirred for 12 h; volatiles were removed under vac., a toluene soln. was slowly evapd.; elem. anal.;
DOI:10.1016/S0020-1693(02)01305-1