tris[4-(2-bis[2-(2-furyl)ethyl]phosphoroselenoylethyl)benzyl]phosphine oxide

Base Information

Chemical Name:tris[4-(2-bis[2-(2-furyl)ethyl]phosphoroselenoylethyl)benzyl]phosphine oxide
CAS No.:1402851-46-0
Molecular Formula:C₆₃H₇₂O₇P₄Se₃
Molecular Weight:1302.04
Hs Code.:

Synonyms:tris[4-(2-bis[2-(2-furyl)ethyl]phosphoroselenoylethyl)benzyl]phosphine oxide

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Chemical Property of tris[4-(2-bis[2-(2-furyl)ethyl]phosphoroselenoylethyl)benzyl]phosphine oxide

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Technology Process of tris[4-(2-bis[2-(2-furyl)ethyl]phosphoroselenoylethyl)benzyl]phosphine oxide

There total 3 articles about tris[4-(2-bis[2-(2-furyl)ethyl]phosphoroselenoylethyl)benzyl]phosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 916773-71-2
tris(4-vinylbanzyl)phosphine oxide

: 1239861-25-6
bis[2-(2-furyl)ethyl]phosphine selenide

: 1402851-46-0
tris[4-(2-bis[2-(2-furyl)ethyl]phosphoroselenoylethyl)benzyl]phosphine oxide

Guidance literature:: In benzene; at 25 - 30 ℃; for 4h; regioselective reaction; Inert atmosphere; UV-irradiation;
DOI:10.1016/j.tet.2012.08.091

Reference yield:

: bis[2-(2-furyl)ethyl]phosphine

: 1402851-46-0
tris[4-(2-bis[2-(2-furyl)ethyl]phosphoroselenoylethyl)benzyl]phosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: selenium / Inert atmosphere

2: benzene / 4 h / 25 - 30 °C / Inert atmosphere; UV-irradiation

With selenium; In benzene;
DOI:10.1016/j.tet.2012.08.091

Reference yield:

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 1402851-46-0
tris[4-(2-bis[2-(2-furyl)ethyl]phosphoroselenoylethyl)benzyl]phosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus; potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water / Inert atmosphere

2: benzene / 4 h / 25 - 30 °C / Inert atmosphere; UV-irradiation

With phosphorus; N-benzyl-N,N,N-triethylammonium chloride; potassium hydroxide; In water; benzene;
DOI:10.1016/j.tet.2012.08.091