(+/-)-3-(6'-acetoxymethyl-2',6'-dimethyl-1'-cyclohexen-1'-yl)-1-methyl-2-propynyl acetate

Base Information

Chemical Name:(+/-)-3-(6'-acetoxymethyl-2',6'-dimethyl-1'-cyclohexen-1'-yl)-1-methyl-2-propynyl acetate
CAS No.:107208-19-5
Molecular Formula:C₁₇H₂₄O₄
Molecular Weight:292.375
Hs Code.:

Synonyms:(+/-)-3-(6'-acetoxymethyl-2',6'-dimethyl-1'-cyclohexen-1'-yl)-1-methyl-2-propynyl acetate

Suppliers and Price of (+/-)-3-(6'-acetoxymethyl-2',6'-dimethyl-1'-cyclohexen-1'-yl)-1-methyl-2-propynyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-3-(6'-acetoxymethyl-2',6'-dimethyl-1'-cyclohexen-1'-yl)-1-methyl-2-propynyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-3-(6'-acetoxymethyl-2',6'-dimethyl-1'-cyclohexen-1'-yl)-1-methyl-2-propynyl acetate

There total 5 articles about (+/-)-3-(6'-acetoxymethyl-2',6'-dimethyl-1'-cyclohexen-1'-yl)-1-methyl-2-propynyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 107208-18-4
(+/-)-3-(6'-acetoxymethyl-1'-hydroxy-2',6'-dimethylcyclohexyl)-1-methyl-2-propynyl acetate

: 107208-19-5
(+/-)-3-(6'-acetoxymethyl-2',6'-dimethyl-1'-cyclohexen-1'-yl)-1-methyl-2-propynyl acetate

Guidance literature:: With trichlorophosphate; In pyridine; at 100 ℃; for 5h;

Reference yield:

: 13756-98-4
(+/-)-2-hydroxymethyl-2,6-dimethyl-1-cyclohexanone

: 107208-19-5
(+/-)-3-(6'-acetoxymethyl-2',6'-dimethyl-1'-cyclohexen-1'-yl)-1-methyl-2-propynyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: p-TsOH / benzene / 3.5 h / Ambient temperature

2: 93 percent / n-BuLi / tetrahydrofuran; hexane / -10 - 0 deg C, 2 h. then room temp.

3: 98 percent / PPTS / ethanol / 4.5 h / 55 °C

4: 94 percent / pyridine / 15 h / Ambient temperature

5: 50 percent / POCl₃ / pyridine / 5 h / 100 °C

With pyridine; n-butyllithium; trichlorophosphate; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; ethanol; hexane; benzene;

Reference yield:

: 107208-15-1
(+/-)-2,6-dimethyl-2-tetrahydropyranyl-oxymethyl-1-cyclohexanone

: 107208-19-5
(+/-)-3-(6'-acetoxymethyl-2',6'-dimethyl-1'-cyclohexen-1'-yl)-1-methyl-2-propynyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / n-BuLi / tetrahydrofuran; hexane / -10 - 0 deg C, 2 h. then room temp.

2: 98 percent / PPTS / ethanol / 4.5 h / 55 °C

3: 94 percent / pyridine / 15 h / Ambient temperature

4: 50 percent / POCl₃ / pyridine / 5 h / 100 °C

With pyridine; n-butyllithium; trichlorophosphate; pyridinium p-toluenesulfonate; In tetrahydrofuran; pyridine; ethanol; hexane;