N-benzyl-N-[(1S)-1-benzyl-2-oxoethyl]-(E)-2-phenyleth-1-ene-1-sulfonamide

Base Information

• Chemical Name: N-benzyl-N-[(1S)-1-benzyl-2-oxoethyl]-(E)-2-phenyleth-1-ene-1-sulfonamide
• CAS No.: 349659-72-9
• Molecular Formula: C₂₄H₂₃NO₃S
• Molecular Weight: 405.518

Synonyms:N-benzyl-N-[(1S)-1-benzyl-2-oxoethyl]-(E)-2-phenyleth-1-ene-1-sulfonamide

Chemical Property of N-benzyl-N-[(1S)-1-benzyl-2-oxoethyl]-(E)-2-phenyleth-1-ene-1-sulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzyl-N-[(1S)-1-benzyl-2-oxoethyl]-(E)-2-phenyleth-1-ene-1-sulfonamide

There total 2 articles about N-benzyl-N-[(1S)-1-benzyl-2-oxoethyl]-(E)-2-phenyleth-1-ene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans 2-phenylethenesulfonyl chloride (52147-97-4) → N-benzyl-N-[(1S)-1-benzyl-2-oxoethyl]-(E)-2-phenyleth-1-ene-1-sulfonamide (349659-72-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / Et₃N / CH₂Cl₂ / 6 h / 25 °C

2: 80 percent / Dess-Martin periodinane; H₂O / CH₂Cl₂ / 0.5 h / 20 °C

With water; Dess-Martin periodane; triethylamine; In dichloromethane;

DOI:10.1016/S0040-4020(01)00186-7

Reference yield:

DL-2-benzylamino-3-phenyl-1-propanol (19881-90-4) → N-benzyl-N-[(1S)-1-benzyl-2-oxoethyl]-(E)-2-phenyleth-1-ene-1-sulfonamide (349659-72-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / Et₃N / CH₂Cl₂ / 6 h / 25 °C

2: 80 percent / Dess-Martin periodinane; H₂O / CH₂Cl₂ / 0.5 h / 20 °C

With water; Dess-Martin periodane; triethylamine; In dichloromethane;

DOI:10.1016/S0040-4020(01)00186-7

Reference yield: 85.0%

N-methylhydroxyamine hydrochloride (4229-44-1) + N-benzyl-N-[(1S)-1-benzyl-2-oxoethyl]-(E)-2-phenyleth-1-ene-1-sulfonamide (349659-72-9) → (3S,3aR,6S,6aS)-5,6-dibenzyl-1-methyl-3-phenylperhydro-4λ6-isothiazolo[4,5-c]isoxazole-4,4-dioxide

Guidance literature:

With triethylamine; In ethanol; for 24h; Heating;

DOI:10.1016/S0040-4020(01)00186-7

upstream raw materials:

trans 2-phenylethenesulfonyl chloride

DL-2-benzylamino-3-phenyl-1-propanol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 349659-72-9 N-benzyl-N-[(1S)-1-benzyl-2-oxoethyl]-(E)-2-phenyleth-1-ene-1-sulfonamide

Send

Send

Metric Ton KG G Pound L ML

Send

Send