1-[(2R,3R,4S,5R)-4-Benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

Base Information

Chemical Name:1-[(2R,3R,4S,5R)-4-Benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione
CAS No.:149774-40-3
Molecular Formula:C₂₆H₂₈N₂O₆Se
Molecular Weight:543.478
Hs Code.:

Synonyms:1-[(2R,3R,4S,5R)-4-Benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

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Chemical Property of 1-[(2R,3R,4S,5R)-4-Benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

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Technology Process of 1-[(2R,3R,4S,5R)-4-Benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

There total 3 articles about 1-[(2R,3R,4S,5R)-4-Benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68144-11-6
1,4-anhydro-2-deoxy-5,6-O-isopropylidene-D-arabinohex-1-enitol

: 149774-40-3
1-[(2R,3R,4S,5R)-4-Benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran

2: 2.) silver trifluoromethanesulfonate / 1.) ether, room temperature, 5 min, 2.) ether, room temperature, 1.5 h

With silver trifluoromethanesulfonate; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(97)00697-2

Reference yield:

: 100-39-0
benzyl bromide

: 149774-40-3
1-[(2R,3R,4S,5R)-4-Benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran

2: 2.) silver trifluoromethanesulfonate / 1.) ether, room temperature, 5 min, 2.) ether, room temperature, 1.5 h

With silver trifluoromethanesulfonate; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(97)00697-2

Reference yield:

: 5707-04-0
Phenylselenyl chloride

: 79241-07-9
(R)-4-((2S,3R)-3-(benzyloxy)-2,3-dihydrofuran-2-yl)-2,2-dimethyl-1,3-dioxolan

: 10457-14-4
O,O'-bis-(trimethylsilyl)uracil

: 1-[(2S,3R,4S,5R)-4-Benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

: 149774-40-3
1-[(2R,3R,4S,5R)-4-Benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

Guidance literature:: With silver trifluoromethanesulfonate; Yield given. Multistep reaction. Yields of byproduct given; 1.) ether, room temperature, 5 min, 2.) ether, room temperature, 1.5 h;
DOI:10.1016/S0040-4020(97)00697-2