3-Iodobenzamide

Base Information

• Chemical Name: 3-Iodobenzamide
• CAS No.: 10388-19-9
• Molecular Formula: C7H6INO
• Molecular Weight: 247.035
• Hs Code.: 2924299090
• DSSTox Substance ID: DTXSID10146125
• Nikkaji Number: J211.366J
• Wikidata: Q83010867
• Mol file: 10388-19-9.mol

Synonyms:3-Iodobenzamide;10388-19-9;Benzamide, 3-iodo-;m-Iodobenzamide;Benzamide, m-iodo-;BRN 2434281;MFCD00143169;0-09-00-00366 (Beilstein Handbook Reference);3-iodo-benzamide;3-iodanylbenzamide;3-Iodobenzamide #;3-Iodobenzoic amide;SCHEMBL1259478;DTXSID10146125;AKOS003635157;AS-16039;LS-27050;SY041741;CS-0213205;FT-0615894;I1035;T71545;PENTAFLUOROETHYL2,2,2-TRIFLUOROETHYLETHER;A800837;Z33546647;F1084-0309

Chemical Property of 3-Iodobenzamide

Chemical Property:

• Vapor Pressure: 0.000278mmHg at 25°C
• Melting Point: 187 °C
• Refractive Index: 1.66
• Boiling Point: 322.5 °C at 760 mmHg
• Flash Point: 148.9 °C
• PSA: 43.09000
• Density: 1.897 g/cm³
• LogP: 2.09040
• Storage Temp.: 2-8°C
• Solubility.: soluble in Dimethylformamide
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 246.94941
• Heavy Atom Count: 10
• Complexity: 138

Purity/Quality:

97% ^*data from raw suppliers

3-Iodobenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)I)C(=O)N

Technology Process of 3-Iodobenzamide

There total 13 articles about 3-Iodobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-Iodobenzoic acid (618-51-9) → m-iodobenzamide (10388-19-9)

Guidance literature:

3-Iodobenzoic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; for 2h;

With ammonia; In tetrahydrofuran; water; for 1.5h;

Reference yield: 98.0%

→ m-iodobenzamide (10388-19-9)

Guidance literature:

Reference yield: 88.0%

benzamide (55-21-0,27208-38-4) → m-iodobenzamide (10388-19-9)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; iodine; In acetic anhydride; acetic acid; at 20 - 45 ℃; for 5h;

DOI:10.1246/bcsj.70.1665

upstream raw materials:

3-iodobenzoyl chloride

benzamide

urea

3-Iodobenzoic acid

Downstream raw materials:

3-({6-[4-(pyridin-3-yloxy)piperidin-1-yl]pyridazin-3-yl}ethynyl)benzamide

3-(6-methoxy-1H-indol-2-yl)benzamide

3-<1-deoxy-2,3-O-(1-methyl-1,1-ethanediyl)-β-D-ribofuranosyl>benzamide