bis(2-phenylethyl) 4-oxoheptanedioate

Base Information

Chemical Name:bis(2-phenylethyl) 4-oxoheptanedioate
CAS No.:211509-33-0
Molecular Formula:C₂₃H₂₆O₅
Molecular Weight:382.456
Hs Code.:

Synonyms:bis(2-phenylethyl) 4-oxoheptanedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(2-phenylethyl) 4-oxoheptanedioate

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Technology Process of bis(2-phenylethyl) 4-oxoheptanedioate

There total 1 articles about bis(2-phenylethyl) 4-oxoheptanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 6317-49-3
4-oxopimelate

: 60-12-8
2-phenylethanol

: 211509-33-0
bis(2-phenylethyl) 4-oxoheptanedioate

Guidance literature:: With sulfuric acid; In toluene; for 5h; Heating;
DOI:10.1139/cjc-76-4-490

Reference yield: 85.0%

: 7550-45-0
titanium tetrachloride

: 211509-33-0
bis(2-phenylethyl) 4-oxoheptanedioate

: (TiCl₄)4(bis(2-phenylethyl) 4-oxoheptanedioate)2 * CH₂Cl₂

Guidance literature:: In dichloromethane; N2-atmosphere; dropwise addn. of 2 equiv. TiCl4 to ligand (25°C, stirring); layering with MeOH, crystn.;
DOI:10.1139/cjc-76-4-490