2-(arylmethylene)-4aβ,8aαH-decahydronaphthalen

Base Information

• Chemical Name: 2-(arylmethylene)-4aβ,8aαH-decahydronaphthalen
• CAS No.: 76178-28-4
• Molecular Formula: C₁₇H₂₂O
• Molecular Weight: 242.361

Synonyms:2-(arylmethylene)-4aβ,8aαH-decahydronaphthalen

Chemical Property of 2-(arylmethylene)-4aβ,8aαH-decahydronaphthalen

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Technology Process of 2-(arylmethylene)-4aβ,8aαH-decahydronaphthalen

There total 2 articles about 2-(arylmethylene)-4aβ,8aαH-decahydronaphthalen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(+/-)-2-((E)-benzyliden)-(4ar,8at)-octahydro-naphthalen-1-one (17429-48-0,59203-29-1,59203-30-4) → 2-(arylmethylene)-4aβ,8aαH-decahydronaphthalen (76178-28-4)

Guidance literature:

With sodium tetrahydroborate; In methanol; water; at 15 - 20 ℃; for 0.333333h;

Reference yield:

(+/-)-2-((E)-benzyliden)-(4ar,8at)-octahydro-naphthalen-1-one (17429-48-0,59203-29-1,59203-30-4) → (+/-)-2-((E)-benzylidene)-(4ar,8at)-decahydro-[1=x]naphthol (76178-28-4)

Guidance literature:

With lithium aluminium tetrahydride;

DOI:10.1021/ja01119a045

Reference yield: 94.0%

acetic anhydride (108-24-7) + 2-(arylmethylene)-4aβ,8aαH-decahydronaphthalen (76178-28-4) → Acetic acid (1S,4aS,8aR)-2-[1-phenyl-meth-(E)-ylidene]-decahydro-naphthalen-1-yl ester (76178-29-5)

Guidance literature:

With pyridine; for 48h; Ambient temperature;

upstream raw materials:

(+/-)-2-((E)-benzyliden)-(4ar,8at)-octahydro-naphthalen-1-one

Downstream raw materials:

Acetic acid (1S,4aS,8aR)-2-[1-phenyl-meth-(E)-ylidene]-decahydro-naphthalen-1-yl ester

Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester

2β-benzoylamino-4aβH,8aαH-decahydronaphthalen-1α-ol

(3aR,5aR,9aS,9bS)-2-Phenyl-3a,4,5,5a,6,7,8,9,9a,9b-decahydro-1-oxa-3-aza-cyclopenta[a]naphthalene

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