(3aR,5aR,9aS,9bS)-2-Phenyl-3a,4,5,5a,6,7,8,9,9a,9b-decahydro-1-oxa-3-aza-cyclopenta[a]naphthalene

Base Information

Chemical Name:(3aR,5aR,9aS,9bS)-2-Phenyl-3a,4,5,5a,6,7,8,9,9a,9b-decahydro-1-oxa-3-aza-cyclopenta[a]naphthalene
CAS No.:76178-36-4
Molecular Formula:C₁₇H₂₁NO
Molecular Weight:255.36
Hs Code.:

Synonyms:

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Chemical Property of (3aR,5aR,9aS,9bS)-2-Phenyl-3a,4,5,5a,6,7,8,9,9a,9b-decahydro-1-oxa-3-aza-cyclopenta[a]naphthalene

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Technology Process of (3aR,5aR,9aS,9bS)-2-Phenyl-3a,4,5,5a,6,7,8,9,9a,9b-decahydro-1-oxa-3-aza-cyclopenta[a]naphthalene

There total 9 articles about (3aR,5aR,9aS,9bS)-2-Phenyl-3a,4,5,5a,6,7,8,9,9a,9b-decahydro-1-oxa-3-aza-cyclopenta[a]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76178-35-3
Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester

: 76178-36-4
(3aR,5aR,9aS,9bS)-2-Phenyl-3a,4,5,5a,6,7,8,9,9a,9b-decahydro-1-oxa-3-aza-cyclopenta[a]naphthalene

Guidance literature:: With potassium acetate; In ethanol; at 90 ℃; for 7h;

Reference yield:

: 17429-48-0,59203-29-1,59203-30-4
(+/-)-2-((E)-benzyliden)-(4ar,8at)-octahydro-naphthalen-1-one

: 76178-36-4
(3aR,5aR,9aS,9bS)-2-Phenyl-3a,4,5,5a,6,7,8,9,9a,9b-decahydro-1-oxa-3-aza-cyclopenta[a]naphthalene

Guidance literature:: Multi-step reaction with 8 steps

1: 98 percent / sodium borohydride / methanol; H₂O / 0.33 h / 15 - 20 °C

2: 94 percent / pyridine / 48 h / Ambient temperature

3: 1.) ozone, 2.) zinc, acetic acid / 1.) ethyl acetate, -64 deg C, 24 h, 2.) ethyl acetate, 30 min

4: 65 percent / pyridine, hydroxylamine hydrochloride / ethanol / 1 h / Heating

5: 65 percent / lithium aluminium hydride / diisopropyl ether; diethyl ether / 15 h / Heating

6: 70 percent / aq. sodium hydroxide / benzene / 0.33 h

7: pyridine / 4 h / Ambient temperature

8: potassium acetate / ethanol / 7 h / 90 °C

With pyridine; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; hydroxylamine hydrochloride; potassium acetate; ozone; acetic acid; zinc; In methanol; diethyl ether; ethanol; di-isopropyl ether; water; benzene;

Reference yield:

: 76178-28-4
2-(arylmethylene)-4aβ,8aαH-decahydronaphthalen

: 76178-36-4
(3aR,5aR,9aS,9bS)-2-Phenyl-3a,4,5,5a,6,7,8,9,9a,9b-decahydro-1-oxa-3-aza-cyclopenta[a]naphthalene

Guidance literature:: Multi-step reaction with 7 steps

1: 94 percent / pyridine / 48 h / Ambient temperature

2: 1.) ozone, 2.) zinc, acetic acid / 1.) ethyl acetate, -64 deg C, 24 h, 2.) ethyl acetate, 30 min

3: 65 percent / pyridine, hydroxylamine hydrochloride / ethanol / 1 h / Heating

4: 65 percent / lithium aluminium hydride / diisopropyl ether; diethyl ether / 15 h / Heating

5: 70 percent / aq. sodium hydroxide / benzene / 0.33 h

6: pyridine / 4 h / Ambient temperature

7: potassium acetate / ethanol / 7 h / 90 °C

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; potassium acetate; ozone; acetic acid; zinc; In diethyl ether; ethanol; di-isopropyl ether; benzene;