Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester

Base Information

Chemical Name:Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester
CAS No.:76178-35-3
Molecular Formula:C₁₈H₂₅NO₄S
Molecular Weight:351.467
Hs Code.:

Synonyms:

Suppliers and Price of Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester

There total 8 articles about Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17429-48-0,59203-29-1,59203-30-4
(+/-)-2-((E)-benzyliden)-(4ar,8at)-octahydro-naphthalen-1-one

: 76178-35-3
Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / sodium borohydride / methanol; H₂O / 0.33 h / 15 - 20 °C

2: 94 percent / pyridine / 48 h / Ambient temperature

3: 1.) ozone, 2.) zinc, acetic acid / 1.) ethyl acetate, -64 deg C, 24 h, 2.) ethyl acetate, 30 min

4: 65 percent / pyridine, hydroxylamine hydrochloride / ethanol / 1 h / Heating

5: 65 percent / lithium aluminium hydride / diisopropyl ether; diethyl ether / 15 h / Heating

6: 70 percent / aq. sodium hydroxide / benzene / 0.33 h

7: pyridine / 4 h / Ambient temperature

With pyridine; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; hydroxylamine hydrochloride; ozone; acetic acid; zinc; In methanol; diethyl ether; ethanol; di-isopropyl ether; water; benzene;

Reference yield:

: 76178-28-4
2-(arylmethylene)-4aβ,8aαH-decahydronaphthalen

: 76178-35-3
Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / pyridine / 48 h / Ambient temperature

2: 1.) ozone, 2.) zinc, acetic acid / 1.) ethyl acetate, -64 deg C, 24 h, 2.) ethyl acetate, 30 min

3: 65 percent / pyridine, hydroxylamine hydrochloride / ethanol / 1 h / Heating

4: 65 percent / lithium aluminium hydride / diisopropyl ether; diethyl ether / 15 h / Heating

5: 70 percent / aq. sodium hydroxide / benzene / 0.33 h

6: pyridine / 4 h / Ambient temperature

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; ozone; acetic acid; zinc; In diethyl ether; ethanol; di-isopropyl ether; benzene;

Reference yield:

: 76178-31-9
1α-acetoxy-4aβH,8aαH-octahydronaphthalen-2(1H)-one

: 76178-35-3
Methanesulfonic acid (1S,2S,4aS,8aR)-2-benzoylamino-decahydro-naphthalen-1-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / pyridine, hydroxylamine hydrochloride / ethanol / 1 h / Heating

2: 65 percent / lithium aluminium hydride / diisopropyl ether; diethyl ether / 15 h / Heating

3: 70 percent / aq. sodium hydroxide / benzene / 0.33 h

4: pyridine / 4 h / Ambient temperature

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; In diethyl ether; ethanol; di-isopropyl ether; benzene;