8-methoxy-2,4-diphenylquinazoline

Base Information

Chemical Name:8-methoxy-2,4-diphenylquinazoline
CAS No.:1026136-95-7
Molecular Formula:C₂₁H₁₆N₂O
Molecular Weight:312.371
Hs Code.:

Synonyms:8-methoxy-2,4-diphenylquinazoline

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Chemical Property of 8-methoxy-2,4-diphenylquinazoline

Chemical Property:

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Technology Process of 8-methoxy-2,4-diphenylquinazoline

There total 4 articles about 8-methoxy-2,4-diphenylquinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1-(tert-butylsulfinyl)-2-methoxybenzene

: 100-47-0
benzonitrile

: 1026136-95-7
8-methoxy-2,4-diphenylquinazoline

Guidance literature:: 1-(tert-butylsulfinyl)-2-methoxybenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

benzonitrile; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1039/b716954j

Reference yield:

: C₂₁H₂₀N₂O

: 1026136-95-7
8-methoxy-2,4-diphenylquinazoline

Guidance literature:: With silver(II) oxide; In Hexafluorobenzene; at 100 ℃; for 12h;
DOI:10.1016/j.tetlet.2018.05.019

Reference yield:

: 5395-00-6
N-(2-methoxyphenyl)benzamide

: 1026136-95-7
8-methoxy-2,4-diphenylquinazoline

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 10 h / Heating

2: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / 80 °C / Molecular sieve

3: silver(II) oxide / Hexafluorobenzene / 12 h / 100 °C

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; silver(II) oxide; thionyl chloride; In Hexafluorobenzene;
DOI:10.1016/j.tetlet.2018.05.019