1,1-bis(4'-hydroxyphenyl)-4-methylcyclohexane

Base Information

• Chemical Name: 1,1-bis(4'-hydroxyphenyl)-4-methylcyclohexane
• CAS No.: 94385-18-9
• Molecular Formula: C₁₉H₂₂O₂
• Molecular Weight: 282.382
• Mol file: 94385-18-9.mol

Synonyms:1,1-bis(4'-hydroxyphenyl)-4-methylcyclohexane

Chemical Property of 1,1-bis(4'-hydroxyphenyl)-4-methylcyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1-bis(4'-hydroxyphenyl)-4-methylcyclohexane

There total 2 articles about 1,1-bis(4'-hydroxyphenyl)-4-methylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1-methylcyclohexan-4-one (589-92-4) + phenol (108-95-2,27073-41-2) → 1,1-bis(4'-hydroxyphenyl)-4-methylcyclohexane (94385-18-9)

Guidance literature:

With hydrogenchloride; cetyltrimethylammonium chloride; 3-mercaptopropionic acid; sodium hydroxide; In water; for 4h;

Reference yield:

→ 1,1-bis(4'-hydroxyphenyl)-4-methylcyclohexane (94385-18-9)

Guidance literature:

Phenol, 4-Methylcyclohexanon, H3PO4 (D: 1.86), Δ;

Reference yield:

1,1-bis(4'-hydroxyphenyl)-4-methylcyclohexane (94385-18-9) → [4-(4-methyl-cyclohex-1-enyl)-phenoxy]-acetic acid

Guidance literature:

Multi-step reaction with 2 steps

1: Pyrolysis

2: aqueous NaOH / auf dem Dampfbad

With sodium hydroxide;

DOI:10.1021/ja01871a032

upstream raw materials:

1-methylcyclohexan-4-one

phenol

Downstream raw materials:

(+/-)-4-hydroxy-1-(4-methyl-cyclohexen-⁽¹⁾-yl)-benzene

phenol

4'-propyloxy-4-biphenylcarboxylic acid

4'-n-pentyloxybiphenyl-4-carboxylic acid