2-methyl-6-morpholino-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

Base Information

Chemical Name:2-methyl-6-morpholino-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide
CAS No.:1300857-16-2
Molecular Formula:C₁₉H₁₅F₇N₂O₂
Molecular Weight:436.329
Hs Code.:

Synonyms:2-methyl-6-morpholino-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

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Chemical Property of 2-methyl-6-morpholino-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

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Technology Process of 2-methyl-6-morpholino-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

There total 4 articles about 2-methyl-6-morpholino-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1300857-03-7
2-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

: 1452757-48-0
N-benzoyloxylmorpholine

: 1300857-16-2
2-methyl-6-morpholino-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

Guidance literature:: With [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium carbonate; In acetone; at 20 ℃; for 36h; Schlenk technique;
DOI:10.1021/ol402515s

Reference yield: 89.0%

: 5765-65-1
4-(benzoyloxy)morpholine

: 1300857-03-7
2-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

: 1300857-16-2
2-methyl-6-morpholino-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

Guidance literature:: With silver(I) acetate; palladium diacetate; cesium fluoride; In 1,2-dichloro-ethane; at 130 ℃; for 18h; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/ja202563w

Reference yield:

: 933-88-0
ortho-toluoyl chloride

: 1300857-16-2
2-methyl-6-morpholino-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 12 h / Reflux

2: silver(I) acetate; palladium diacetate; cesium fluoride / 1,2-dichloro-ethane / 18 h / 130 °C / 760.05 Torr / Inert atmosphere

With silver(I) acetate; palladium diacetate; cesium fluoride; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/ja202563w