N₂-(3,5-dimethoxyphenyl)-N₄,N₄-dimethyl-6-(prop-2-ynyloxy)-1,3,5-triazine-2,4-diamine

Base Information

• Chemical Name: N₂-(3,5-dimethoxyphenyl)-N₄,N₄-dimethyl-6-(prop-2-ynyloxy)-1,3,5-triazine-2,4-diamine
• CAS No.: 1335447-90-9
• Molecular Formula: C₁₆H₁₉N₅O₃
• Molecular Weight: 329.359

Synonyms:N₂-(3,5-dimethoxyphenyl)-N₄,N₄-dimethyl-6-(prop-2-ynyloxy)-1,3,5-triazine-2,4-diamine

Chemical Property of N₂-(3,5-dimethoxyphenyl)-N₄,N₄-dimethyl-6-(prop-2-ynyloxy)-1,3,5-triazine-2,4-diamine

Chemical Property:

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Technology Process of N₂-(3,5-dimethoxyphenyl)-N₄,N₄-dimethyl-6-(prop-2-ynyloxy)-1,3,5-triazine-2,4-diamine

There total 3 articles about N₂-(3,5-dimethoxyphenyl)-N₄,N₄-dimethyl-6-(prop-2-ynyloxy)-1,3,5-triazine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(4-chloro-6-prop-2-ynyloxy-[1,3,5]triazin-2-yl)-(3,5-dimethoxyphenyl)amine (1335447-86-3) + dimethyl amine (124-40-3) → N2-(3,5-dimethoxyphenyl)-N4,N4-dimethyl-6-(prop-2-ynyloxy)-1,3,5-triazine-2,4-diamine (1335447-90-9)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1111/j.1747-0285.2011.01115.x

Reference yield:

3.5-dimethoxyaniline (10272-07-8) → N2-(3,5-dimethoxyphenyl)-N4,N4-dimethyl-6-(prop-2-ynyloxy)-1,3,5-triazine-2,4-diamine (1335447-90-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / tetrahydrofuran / 0 - 5 °C

2: potassium carbonate / tetrahydrofuran / 20 °C

3: tetrahydrofuran / 4 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran;

DOI:10.1111/j.1747-0285.2011.01115.x

Reference yield:

(4,6-dichloro-[1,3,5]triazin-2-yl)-(3,5-dimethoxyphenyl)amine (1284193-14-1) → N2-(3,5-dimethoxyphenyl)-N4,N4-dimethyl-6-(prop-2-ynyloxy)-1,3,5-triazine-2,4-diamine (1335447-90-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran / 20 °C

2: tetrahydrofuran / 4 h / 20 °C

With potassium carbonate; In tetrahydrofuran;

DOI:10.1111/j.1747-0285.2011.01115.x

upstream raw materials:

(4,6-dichloro-[1,3,5]triazin-2-yl)-(3,5-dimethoxyphenyl)amine

(4-chloro-6-prop-2-ynyloxy-[1,3,5]triazin-2-yl)-(3,5-dimethoxyphenyl)amine

dimethyl amine

3.5-dimethoxyaniline

Downstream raw materials:

6-((1-(2-(7-chloroquinolin-4-ylamino)ethyl)-1H-1,2,3-triazol-4-yl)methoxy)-N₂-(3,5-dimethoxyphenyl)-N₄,N₄-dimethyl-1,3,5-triazine-2,4-diamine

6-((1-(3-(7-chloroquinolin-4-ylamino)propyl)-1H-1,2,3-triazol-4-yl)methoxy)-N₂-(3,5-dimethoxyphenyl)-N₄,N₄-dimethyl-1,3,5-triazine-2,4-diamine

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