3-cyclopropyl-5-(p-tolyl)-4H-1,2,4-triazole

Base Information

Chemical Name:3-cyclopropyl-5-(p-tolyl)-4H-1,2,4-triazole
CAS No.:1251249-97-4
Molecular Formula:C₁₂H₁₃N₃
Molecular Weight:199.255
Hs Code.:

Synonyms:3-cyclopropyl-5-(p-tolyl)-4H-1,2,4-triazole

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Chemical Property of 3-cyclopropyl-5-(p-tolyl)-4H-1,2,4-triazole

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Technology Process of 3-cyclopropyl-5-(p-tolyl)-4H-1,2,4-triazole

There total 2 articles about 3-cyclopropyl-5-(p-tolyl)-4H-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 57297-29-7,477904-80-6
cyclopropylcarboxamidine hydrochloride

: 6326-27-8
p-methylbenzamidine hydrochloride

: 1251249-97-4
3-cyclopropyl-5-(p-tolyl)-4H-1,2,4-triazole

Guidance literature:: cyclopropylcarboxamidine hydrochloride; p-methylbenzamidine hydrochloride; With copper; caesium carbonate; In dimethyl sulfoxide; at 120 ℃; for 24h; Inert atmosphere;

With oxygen; In dimethyl sulfoxide; at 120 ℃; for 48h; under 750.075 Torr;
DOI:10.1055/s-0032-1317692

Reference yield:

: 51285-13-3
cyclopropanecarboxamide oxime

: 104-85-8
para-methylbenzonitrile

: 1251249-97-4
3-cyclopropyl-5-(p-tolyl)-4H-1,2,4-triazole

Guidance literature:: With copper diacetate; caesium carbonate; sodium sulfate; In dimethyl sulfoxide; butan-1-ol; at 120 ℃; for 24h; Reagent/catalyst; Temperature; Solvent; Schlenk technique;
DOI:10.1021/jo502709t