N-(2-chloro)phenoxyphthalimide

Base Information

Chemical Name:N-(2-chloro)phenoxyphthalimide
CAS No.:1079392-31-6
Molecular Formula:C₁₄H₈ClNO₃
Molecular Weight:273.675
Hs Code.:

Synonyms:N-(2-chloro)phenoxyphthalimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-chloro)phenoxyphthalimide

Chemical Property:

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Technology Process of N-(2-chloro)phenoxyphthalimide

There total 3 articles about N-(2-chloro)phenoxyphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 524-38-9
N-hydroxyphthalimide

: bis-(2-chlorophenyl)iodonium tetrafluoroborate

: 1079392-31-6
N-(2-chloro)phenoxyphthalimide

Guidance literature:: N-hydroxyphthalimide; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.166667h;

bis-(2-chlorophenyl)iodonium tetrafluoroborate; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1055/s-0033-1340192

Reference yield: 14.0%

: 524-38-9
N-hydroxyphthalimide

: 3900-89-8
2-Chlorobenzeneboronic acid

: 1079392-31-6
N-(2-chloro)phenoxyphthalimide

Guidance literature:: With pyridine; copper(l) chloride; In dichloromethane; for 19h; Molecular sieve; Inert atmosphere;

Reference yield:

: 3900-89-8
2-Chlorobenzeneboronic acid

: 1079392-31-6
N-(2-chloro)phenoxyphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane

2.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 20 °C

2.2: 2 h / 20 °C

With potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0033-1340192