O-(2-chlorophenyl)hydroxylamine

Base Information

Chemical Name:O-(2-chlorophenyl)hydroxylamine
CAS No.:99907-85-4
Molecular Formula:C₆H₆ClNO
Molecular Weight:143.573
Hs Code.:
European Community (EC) Number:822-939-2
DSSTox Substance ID:DTXSID801303538

Synonyms:O-(2-chlorophenyl)hydroxylamine;99907-85-4;SCHEMBL5014006;DTXSID801303538;MFCD25969835;SY282090;CS-0457856;EN300-185064

Suppliers and Price of O-(2-chlorophenyl)hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of O-(2-chlorophenyl)hydroxylamine

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:143.0137915
Heavy Atom Count:9
Complexity:89.1

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)ON)Cl

Technology Process of O-(2-chlorophenyl)hydroxylamine

There total 5 articles about O-(2-chlorophenyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.8%

: N-(2-Chloro-phenoxy)-acetimidic acid ethyl ester

: 99907-85-4
O-(o-chloro-phenyl)-hydroxylamine

Guidance literature:: With perchloric acid; In 1,4-dioxane; for 1h; Ambient temperature;
DOI:10.1080/00304949709355240

Reference yield:

: 1079392-31-6
N-(2-chloro)phenoxyphthalimide

: 99907-85-4
O-(o-chloro-phenyl)-hydroxylamine

Guidance literature:: With ammonia; In methanol; at 20 ℃;
DOI:10.1016/j.bmcl.2008.07.118

Reference yield:

: 3900-89-8
2-Chlorobenzeneboronic acid

: 99907-85-4
O-(o-chloro-phenyl)-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) chloride; pyridine / 1,2-dichloro-ethane / 20 °C / Molecular sieve

2: hydrazine hydrate / methanol; chloroform / 1 h / 20 °C

With pyridine; hydrazine hydrate; copper(l) chloride; In methanol; chloroform; 1,2-dichloro-ethane;
DOI:10.1039/c5cc00354g