tert-butyl (3-{[(4-amino-2-fluorophenyl)carbonyl](methyl)amino}propyl)methylcarbamate

Base Information

Chemical Name:tert-butyl (3-{[(4-amino-2-fluorophenyl)carbonyl](methyl)amino}propyl)methylcarbamate
CAS No.:1246246-95-6
Molecular Formula:C₁₇H₂₆FN₃O₃
Molecular Weight:339.41
Hs Code.:

Synonyms:tert-butyl (3-{[(4-amino-2-fluorophenyl)carbonyl](methyl)amino}propyl)methylcarbamate

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Chemical Property of tert-butyl (3-{[(4-amino-2-fluorophenyl)carbonyl](methyl)amino}propyl)methylcarbamate

Chemical Property:

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Technology Process of tert-butyl (3-{[(4-amino-2-fluorophenyl)carbonyl](methyl)amino}propyl)methylcarbamate

There total 3 articles about tert-butyl (3-{[(4-amino-2-fluorophenyl)carbonyl](methyl)amino}propyl)methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1246246-94-5
tert-Butyl (3-{[(2-fluoro-4-nitrophenyl)carbonyl](methyl)amino}propyl)methylcarbamate

: 1246246-95-6
tert-butyl (3-{[(4-amino-2-fluorophenyl)carbonyl](methyl)amino}propyl)methylcarbamate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 1h;

Reference yield:

: 403-24-7
2-fluoro-4-nitrobenzoic acid

: 1246246-95-6
tert-butyl (3-{[(4-amino-2-fluorophenyl)carbonyl](methyl)amino}propyl)methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; pivaloyl chloride / dichloromethane / 0.25 h / 20 °C / Cooling with ice

1.2: 2 h / 20 °C / Cooling with ice

2.1: hydrogen / palladium 10% on activated carbon / methanol / 1 h / 20 °C

With hydrogen; pivaloyl chloride; triethylamine; palladium 10% on activated carbon; In methanol; dichloromethane;

Reference yield:

: 123183-72-2
N-(tert-butyl)oxycarbonyl-N,N’-trimethyl-1,3-diaminopropane

: 1246246-95-6
tert-butyl (3-{[(4-amino-2-fluorophenyl)carbonyl](methyl)amino}propyl)methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; pivaloyl chloride / dichloromethane / 0.25 h / 20 °C / Cooling with ice

1.2: 2 h / 20 °C / Cooling with ice

2.1: hydrogen / palladium 10% on activated carbon / methanol / 1 h / 20 °C

With hydrogen; pivaloyl chloride; triethylamine; palladium 10% on activated carbon; In methanol; dichloromethane;