C₃₆H₃₄Cl₃NO₁₁

Base Information

Chemical Name:C₃₆H₃₄Cl₃NO₁₁
CAS No.:1577227-81-6
Molecular Formula:C₃₆H₃₄Cl₃NO₁₁
Molecular Weight:763.025
Hs Code.:

C<sub>36</sub>H<sub>34</sub>Cl<sub>3</sub>NO<sub>11</sub>

Synonyms:C₃₆H₃₄Cl₃NO₁₁

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₃₄Cl₃NO₁₁

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Technology Process of C₃₆H₃₄Cl₃NO₁₁

There total 7 articles about C₃₆H₃₄Cl₃NO₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₃₄O₁₁

: 545-06-2
trichloroacetonitrile

: 1577227-81-6
C₃₆H₃₄Cl₃NO₁₁

Guidance literature:: With sodium hydride; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1039/c3ob42312c

Reference yield:

: 1577227-58-7
dimethylthexylsilyl 3-O-benzyl-4,6-di-O-benzylidene-β-D-glucopyranoside

: 1577227-81-6
C₃₆H₃₄Cl₃NO₁₁

Guidance literature:: Multi-step reaction with 6 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane; water / 0.5 h / 20 °C / Inert atmosphere

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: dmap / dichloromethane / 20 °C / Inert atmosphere

5.1: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / Inert atmosphere

6.1: sodium hydride / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; sodium hydride; pyridine hydrogenfluoride; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c3ob42312c

Reference yield:

: 1577227-76-9
dimethylthexylsilyl O-methyl-2-O-levulinoyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate

: 1577227-81-6
C₃₆H₃₄Cl₃NO₁₁

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / Inert atmosphere

2: sodium hydride / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With sodium hydride; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3ob42312c