dimethylthexylsilyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Base Information

Chemical Name:dimethylthexylsilyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside
CAS No.:1577227-60-1
Molecular Formula:C₃₃H₄₆O₈Si
Molecular Weight:598.809
Hs Code.:

Synonyms:dimethylthexylsilyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethylthexylsilyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

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Technology Process of dimethylthexylsilyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

There total 1 articles about dimethylthexylsilyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1577227-58-7
dimethylthexylsilyl 3-O-benzyl-4,6-di-O-benzylidene-β-D-glucopyranoside

: 123-76-2
levulinic acid

: 1577227-60-1
dimethylthexylsilyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3ob42312c

Reference yield: 81.0%

: 1577227-60-1
dimethylthexylsilyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

: 1577227-66-7
dimethylthexylsilyl 2-O-levulinoyl-3-O-benzyl-β-D-glucopyranoside

Guidance literature:: With trifluoroacetic acid; In dichloromethane; water; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c3ob42312c

Reference yield:

: 1577227-60-1
dimethylthexylsilyl 2-O-levulinoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

: 1577227-76-9
dimethylthexylsilyl O-methyl-2-O-levulinoyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane; water / 0.5 h / 20 °C / Inert atmosphere

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: dmap / dichloromethane / 20 °C / Inert atmosphere

With dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; trifluoroacetic acid; In dichloromethane; water;
DOI:10.1039/c3ob42312c