(4R,5S)-(+)-3-[(2R)-2-isopropyl-5-methyl-1-oxohex-5-en-1-yl]-4-methyl-5-phenyl-2-oxazolidinone

Base Information

Chemical Name:(4R,5S)-(+)-3-[(2R)-2-isopropyl-5-methyl-1-oxohex-5-en-1-yl]-4-methyl-5-phenyl-2-oxazolidinone
CAS No.:317801-57-3
Molecular Formula:C₂₀H₂₇NO₃
Molecular Weight:329.439
Hs Code.:

Synonyms:(4R,5S)-(+)-3-[(2R)-2-isopropyl-5-methyl-1-oxohex-5-en-1-yl]-4-methyl-5-phenyl-2-oxazolidinone

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Chemical Property of (4R,5S)-(+)-3-[(2R)-2-isopropyl-5-methyl-1-oxohex-5-en-1-yl]-4-methyl-5-phenyl-2-oxazolidinone

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Technology Process of (4R,5S)-(+)-3-[(2R)-2-isopropyl-5-methyl-1-oxohex-5-en-1-yl]-4-methyl-5-phenyl-2-oxazolidinone

There total 1 articles about (4R,5S)-(+)-3-[(2R)-2-isopropyl-5-methyl-1-oxohex-5-en-1-yl]-4-methyl-5-phenyl-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 109-72-8,29786-93-4
n-butyllithium

: 107599-99-5
(4R,5S)-(+)-3-[3-methyl-1-oxobut-1-yl]-4-methyl-5-phenyl-2-oxazolidinone

: 154106-15-7
3-methylbut-3-en-1-yl trifluoromethanesulphonate

: 317801-57-3
(4R,5S)-(+)-3-[(2R)-2-isopropyl-5-methyl-1-oxohex-5-en-1-yl]-4-methyl-5-phenyl-2-oxazolidinone

: (4R,5S)-(+)-3-[(Z)-2,8-dimethyl-5-oxanona-1,6-dien-6-yl]-4-methyl-5-phenyl-2-oxazolidinone

Guidance literature:: n-butyllithium; (4R,5S)-(+)-3-[3-methyl-1-oxobut-1-yl]-4-methyl-5-phenyl-2-oxazolidinone; With diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

3-methylbut-3-en-1-yl trifluoromethanesulphonate; In tetrahydrofuran; hexane; dichloromethane; at -20 ℃; for 2h;
DOI:10.1016/S0957-4166(00)00316-5

Reference yield: 82.0%

: 317801-57-3
(4R,5S)-(+)-3-[(2R)-2-isopropyl-5-methyl-1-oxohex-5-en-1-yl]-4-methyl-5-phenyl-2-oxazolidinone

: 1117-97-1
N,0-dimethylhydroxylamine

: (1S,2R,5R)-(+)-N,O-dimethyl-3-aza-2,8-dimethyl-5-(1-methylethyl)-4-oxo-1-phenyl-8-nonenyl hydroxyl carboxy imide

Guidance literature:: With trimethylaluminum; In dichloromethane; toluene; at 0 ℃; for 1h;
DOI:10.1016/S0957-4166(00)00316-5

Reference yield: 75.0%

: 317801-57-3
(4R,5S)-(+)-3-[(2R)-2-isopropyl-5-methyl-1-oxohex-5-en-1-yl]-4-methyl-5-phenyl-2-oxazolidinone

: 77943-39-6
4-methyl-5-phenyloxazolidin-2-one

: 317801-61-9
(R)-(+)-2-isopropyl-5-methylhex-5-ene-1-carboxylic acid

Guidance literature:: With lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; at 20 ℃; for 16h;
DOI:10.1016/S0957-4166(00)00316-5