3-[2,7-bis(pent-4-enyloxy)naphthyl]-1-[2,6-bis(pent-4-enyloxy)phenyl]-4,4-dimethyl-4,5-imidazolinium chloride

Base Information

Chemical Name:3-[2,7-bis(pent-4-enyloxy)naphthyl]-1-[2,6-bis(pent-4-enyloxy)phenyl]-4,4-dimethyl-4,5-imidazolinium chloride
CAS No.:1277176-02-9
Molecular Formula:C₄₁H₅₃N₂O₄*Cl
Molecular Weight:673.336
Hs Code.:

Synonyms:3-[2,7-bis(pent-4-enyloxy)naphthyl]-1-[2,6-bis(pent-4-enyloxy)phenyl]-4,4-dimethyl-4,5-imidazolinium chloride

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Chemical Property of 3-[2,7-bis(pent-4-enyloxy)naphthyl]-1-[2,6-bis(pent-4-enyloxy)phenyl]-4,4-dimethyl-4,5-imidazolinium chloride

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Technology Process of 3-[2,7-bis(pent-4-enyloxy)naphthyl]-1-[2,6-bis(pent-4-enyloxy)phenyl]-4,4-dimethyl-4,5-imidazolinium chloride

There total 3 articles about 3-[2,7-bis(pent-4-enyloxy)naphthyl]-1-[2,6-bis(pent-4-enyloxy)phenyl]-4,4-dimethyl-4,5-imidazolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1277176-01-8
2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane

: 122-51-0
orthoformic acid triethyl ester

: 1277176-02-9
3-[2,7-bis(pent-4-enyloxy)naphthyl]-1-[2,6-bis(pent-4-enyloxy)phenyl]-4,4-dimethyl-4,5-imidazolinium chloride

Guidance literature:: 2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane; With hydrogenchloride; In 1,4-dioxane; water; for 0.166667h;

orthoformic acid triethyl ester; at 140 ℃; for 1h;
DOI:10.1002/ejoc.201001367

Reference yield:

: 935431-27-9
1,3-bis(pent-4-enyloxy)aniline

: 1277176-02-9
3-[2,7-bis(pent-4-enyloxy)naphthyl]-1-[2,6-bis(pent-4-enyloxy)phenyl]-4,4-dimethyl-4,5-imidazolinium chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 1.5 h / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil

2.2: 18 h / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / Reflux

3.2: 18 h / 20 °C

4.1: hydrogenchloride / 1,4-dioxane; water / 0.17 h

4.2: 1 h / 140 °C

With hydrogenchloride; lithium aluminium tetrahydride; sodium hydride; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; mineral oil;
DOI:10.1002/ejoc.201001367

Reference yield:

: 1277175-99-1
N-[2,6-bis(pent-4-enyloxy)phenyl]-2-bromo-2-methylpropanamide

: 1277176-02-9
3-[2,7-bis(pent-4-enyloxy)naphthyl]-1-[2,6-bis(pent-4-enyloxy)phenyl]-4,4-dimethyl-4,5-imidazolinium chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil

1.2: 18 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / Reflux

2.2: 18 h / 20 °C

3.1: hydrogenchloride / 1,4-dioxane; water / 0.17 h

3.2: 1 h / 140 °C

With hydrogenchloride; lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; 1,4-dioxane; water; mineral oil;
DOI:10.1002/ejoc.201001367