2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane

Base Information

Chemical Name:2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane
CAS No.:1277176-01-8
Molecular Formula:C₄₀H₅₄N₂O₄
Molecular Weight:626.88
Hs Code.:

Synonyms:2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane

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Chemical Property of 2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane

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Technology Process of 2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane

There total 3 articles about 2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1277175-99-1
N-[2,6-bis(pent-4-enyloxy)phenyl]-2-bromo-2-methylpropanamide

: 1277176-00-7
N-[2,6-bis(pent-4-enyloxy)phenyl]-2-[2,7-bis(pent-4-enyloxy)naphthylamino]-2-methylpropanamide

: 1277176-01-8
2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane

Guidance literature:: N-[2,6-bis(pent-4-enyloxy)phenyl]-2-[2,7-bis(pent-4-enyloxy)naphthylamino]-2-methylpropanamide; With lithium aluminium tetrahydride; In tetrahydrofuran; for 16h; Reflux;

N-[2,6-bis(pent-4-enyloxy)phenyl]-2-bromo-2-methylpropanamide; In tetrahydrofuran; mineral oil; at 20 ℃; for 18h;
DOI:10.1002/ejoc.201001367

Reference yield:

: 935431-27-9
1,3-bis(pent-4-enyloxy)aniline

: 1277176-01-8
2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 1.5 h / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil

2.2: 18 h / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / Reflux

3.2: 18 h / 20 °C

With lithium aluminium tetrahydride; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1002/ejoc.201001367

Reference yield:

: 1277175-99-1
N-[2,6-bis(pent-4-enyloxy)phenyl]-2-bromo-2-methylpropanamide

: 1277176-01-8
2-[2,7-bis(pent-4-enyloxy)naphthylamino]-3-[2,6-bis(pent-4-enyloxy)phenylamino]-2-methylpropane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil

1.2: 18 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / Reflux

2.2: 18 h / 20 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1002/ejoc.201001367