C₁₀H₈ClF₃O₂

Base Information

Chemical Name:C₁₀H₈ClF₃O₂
CAS No.:1541198-34-8
Molecular Formula:C₁₀H₈ClF₃O₂
Molecular Weight:252.621
Hs Code.:

C<sub>10</sub>H<sub>8</sub>ClF<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₀H₈ClF₃O₂

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Chemical Property of C₁₀H₈ClF₃O₂

Chemical Property:

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Technology Process of C₁₀H₈ClF₃O₂

There total 4 articles about C₁₀H₈ClF₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1541198-33-7
C₁₂H₁₂ClF₃O₃

: 1541198-34-8
C₁₀H₈ClF₃O₂

Guidance literature:: With toluene-4-sulfonic acid; In acetone; at 20 ℃; for 5h; Inert atmosphere;

Reference yield:

: 14862-52-3
1,3-dibromo-5-chlorobenzene

: 1541198-34-8
C₁₀H₈ClF₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / hexane; di-isopropyl ether / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Dean-Stark

3.1: tert.-butyl lithium / hexane; di-isopropyl ether / 0.5 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -30 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / acetone / 5 h / 20 °C / Inert atmosphere

With n-butyllithium; tert.-butyl lithium; toluene-4-sulfonic acid; In hexane; di-isopropyl ether; acetone; toluene;

Reference yield:

: 188813-05-0
3-bromo-5-chloro-benzaldehyde

: 1541198-34-8
C₁₀H₈ClF₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Dean-Stark

2.1: tert.-butyl lithium / hexane; di-isopropyl ether / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -30 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid / acetone / 5 h / 20 °C / Inert atmosphere

With tert.-butyl lithium; toluene-4-sulfonic acid; In hexane; di-isopropyl ether; acetone; toluene;