tribenzylgallium

Base Information

Chemical Name:tribenzylgallium
CAS No.:18797-34-7
Molecular Formula:C₂₁H₂₁Ga
Molecular Weight:343.121
Hs Code.:

Synonyms:tribenzylgallium

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Chemical Property of tribenzylgallium

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Technology Process of tribenzylgallium

There total 1 articles about tribenzylgallium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 13450-90-3
Gallium trichloride

: 6921-34-2
benzylmagnesium chloride

: 18797-34-7
tribenzylgallium

Guidance literature:: In diethyl ether; byproducts: MgCl2; addn. of Grignard-soln. to Ga-soln. at room temp. within 60 min, stirring for 2 h; evapn. of solvent, treatment of residue with toluene, filtn., evapn., dissolution of solid (pentane/toluene), cooling of soln., pptn., elem. anal.;

Reference yield: 99.0%

: 18797-34-7
tribenzylgallium

: 13450-90-3
Gallium trichloride

: 304854-91-9
C₆H₅CH₂GaCl₂

Guidance literature:: In toluene; uner Ar; stoich. amts. of compounds stirred at 20°C for 48 h in toluene; solvent evapd. in vac.;
DOI:10.1002/1521-3749(200009)626:9<2028::AID-ZAAC2028>3.0.CO;2-9

Reference yield: 97.0%

: 18797-34-7
tribenzylgallium

: {(C₆H₅CH₂)2Ga(OCH₂C₆H₅)}2

Guidance literature:: With O₂; In toluene; dry O2 is passed through a soln. of Ga-compd. at -78°C (15 min), slow heating to room temp.; evapn. of solvent, crystn. of oil, dissolution of solid in pentane/toluene, filtn., crystn., elem. anal.;