6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione

Base Information

• Chemical Name: 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione
• CAS No.: 97651-04-2
• Molecular Formula: C₁₆H₁₆N₂O₂S
• Molecular Weight: 300.381

Synonyms:6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione

Chemical Property of 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione

Chemical Property:

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Technology Process of 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione

There total 1 articles about 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

piperidinium salt of 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(1H)-thiol (111835-46-2) → 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione (97651-04-2)

Guidance literature:

With hydrogenchloride; In ethanol; Heating;

DOI:10.1007/BF00505906

Reference yield: 84.0%

piperidine (110-89-4) + 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione (97651-04-2) → piperidinium salt of 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(1H)-thiol (111835-46-2)

Guidance literature:

In ethanol;

DOI:10.1007/BF00505906

Reference yield: 79.0%

iodacetamide (144-48-9) + 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-3,4-dihydropyridine-2(1H)-thione (97651-04-2) → 2-carbamoylmethylthio-6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine (111853-33-9)

Guidance literature:

With piperidine; In ethanol;

DOI:10.1007/s10593-005-0156-x

upstream raw materials:

piperidinium salt of 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(1H)-thiol

Downstream raw materials:

piperidinium salt of 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(1H)-thiol

3-amino-6-methyl-4-phenyl-5-ethoxycarbonyl-2-carbamoyl-4,7-dihydrothieno<2,3-b>pyridine

2,2'-bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methylpyridyl) disulfide

2-carbamoylmethylthio-6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine

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