4-Methyl-N-[2-(4-oxo-6-oxa-bicyclo[3.1.0]hex-1-yl)-ethyl]-benzenesulfonamide

Base Information

• Chemical Name: 4-Methyl-N-[2-(4-oxo-6-oxa-bicyclo[3.1.0]hex-1-yl)-ethyl]-benzenesulfonamide
• CAS No.: 176515-90-5
• Molecular Formula: C₁₄H₁₇NO₄S
• Molecular Weight: 295.359

Synonyms:4-Methyl-N-[2-(4-oxo-6-oxa-bicyclo[3.1.0]hex-1-yl)-ethyl]-benzenesulfonamide

Chemical Property of 4-Methyl-N-[2-(4-oxo-6-oxa-bicyclo[3.1.0]hex-1-yl)-ethyl]-benzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 4-Methyl-N-[2-(4-oxo-6-oxa-bicyclo[3.1.0]hex-1-yl)-ethyl]-benzenesulfonamide

There total 2 articles about 4-Methyl-N-[2-(4-oxo-6-oxa-bicyclo[3.1.0]hex-1-yl)-ethyl]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Methyl-N-[2-(3-oxo-cyclopent-1-enyl)-ethyl]-benzenesulfonamide (168908-04-1) → 4-Methyl-N-[2-(4-oxo-6-oxa-bicyclo[3.1.0]hex-1-yl)-ethyl]-benzenesulfonamide (176515-90-5)

Guidance literature:

With hydroxide; dihydrogen peroxide;

DOI:10.1016/0040-4039(96)00390-5

Reference yield:

γ-methoxyallylsulfonyl anion → 4-Methyl-N-[2-(4-oxo-6-oxa-bicyclo[3.1.0]hex-1-yl)-ethyl]-benzenesulfonamide (176515-90-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.) silica gel / 2.) H₂O

2: H₂O₂, OH^(1-)

With hydroxide; dihydrogen peroxide; silica gel;

DOI:10.1016/0040-4039(96)00390-5

Reference yield: 90.0%

phenylhydrazine (100-63-0) + 4-Methyl-N-[2-(4-oxo-6-oxa-bicyclo[3.1.0]hex-1-yl)-ethyl]-benzenesulfonamide (176515-90-5) → N-[2-(1-Hydroxy-3-phenylazo-cyclopent-2-enyl)-ethyl]-4-methyl-benzenesulfonamide

Guidance literature:

With camphor-10-sulfonic acid; In chloroform-d1; at 25 ℃;

DOI:10.1016/0040-4039(96)00390-5

upstream raw materials:

4-Methyl-N-[2-(3-oxo-cyclopent-1-enyl)-ethyl]-benzenesulfonamide

Downstream raw materials:

1-(Toluene-4-sulfonyl)-2,3,4,5-tetrahydro-1H-cyclopenta[b]pyrrol-6-one

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