N-<(1-((2,2-dimethylpropanoyl)oxy)cyclohexyl)-methylidene>cyclohexanamine

Base Information

Chemical Name:N-<(1-((2,2-dimethylpropanoyl)oxy)cyclohexyl)-methylidene>cyclohexanamine
CAS No.:100812-02-0
Molecular Formula:C₁₈H₃₁NO₂
Molecular Weight:293.45
Hs Code.:

Synonyms:N-<(1-((2,2-dimethylpropanoyl)oxy)cyclohexyl)-methylidene>cyclohexanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(1-((2,2-dimethylpropanoyl)oxy)cyclohexyl)-methylidene>cyclohexanamine

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Technology Process of N-<(1-((2,2-dimethylpropanoyl)oxy)cyclohexyl)-methylidene>cyclohexanamine

There total 3 articles about N-<(1-((2,2-dimethylpropanoyl)oxy)cyclohexyl)-methylidene>cyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 3282-30-2
pivaloyl chloride

: 60795-42-8
N-(cyclohexylmethylidene)cyclohexanamine N-oxide

: 100812-02-0
N-<(1-((2,2-dimethylpropanoyl)oxy)cyclohexyl)-methylidene>cyclohexanamine

Guidance literature:: With triethylamine; In diethyl ether; for 2h; Ambient temperature;
DOI:10.1021/jo00359a002

Reference yield:

: 25100-12-3
N-cyclohexylhydroxylamine hydrochloride

: 100812-02-0
N-<(1-((2,2-dimethylpropanoyl)oxy)cyclohexyl)-methylidene>cyclohexanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / CH₃COONa / H₂O; ethanol / 24 h / Ambient temperature

2: 93 percent / triethylamine / diethyl ether / 2 h / Ambient temperature

With sodium acetate; triethylamine; In diethyl ether; ethanol; water;
DOI:10.1021/jo00359a002

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 100812-02-0
N-<(1-((2,2-dimethylpropanoyl)oxy)cyclohexyl)-methylidene>cyclohexanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / CH₃COONa / H₂O; ethanol / 24 h / Ambient temperature

2: 93 percent / triethylamine / diethyl ether / 2 h / Ambient temperature

With sodium acetate; triethylamine; In diethyl ether; ethanol; water;
DOI:10.1021/jo00359a002