C₁₉H₂₈O₄SSi

Base Information

Chemical Name:C₁₉H₂₈O₄SSi
CAS No.:1290051-00-1
Molecular Formula:C₁₉H₂₈O₄SSi
Molecular Weight:380.58
Hs Code.:

C<sub>19</sub>H<sub>28</sub>O<sub>4</sub>SSi

Synonyms:C₁₉H₂₈O₄SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₂₈O₄SSi

Chemical Property:

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Technology Process of C₁₉H₂₈O₄SSi

There total 6 articles about C₁₉H₂₈O₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₈O₃SSi

: 1290051-12-5
C₁₉H₂₈O₄SSi

: 1290051-00-1
C₁₉H₂₈O₄SSi

Guidance literature:: With Oxone; 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate; In water; acetonitrile; at 8 - 10 ℃; for 3h; optical yield given as %de;
DOI:10.1039/c0cc05405d

Reference yield:

: 882-33-7
diphenyldisulfane

: 1290051-12-5
C₁₉H₂₈O₄SSi

: 1290051-00-1
C₁₉H₂₈O₄SSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

1.2: 6 h / 20 °C / Inert atmosphere

2.1: trimethylsilyl trifluoromethanesulfonate; triethylamine / dichloromethane / 8 h / Inert atmosphere; Reflux

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

5.1: Oxone; 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate / water; acetonitrile / 3 h / 8 - 10 °C

With Oxone; 1,1,1-trifluoro-2-propanone; trimethylsilyl trifluoromethanesulfonate; sodium hexamethyldisilazane; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1039/c0cc05405d

Reference yield:

: 476331-49-4
(1R,6R)-2-(phenylsulfonyl)-7-oxabicyclo[4.1.0]hept-2-ene

: 1290051-12-5
C₁₉H₂₈O₄SSi

: 1290051-00-1
C₁₉H₂₈O₄SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: water / hexane; dichloromethane / 1.5 h / -20 °C / Inert atmosphere

1.2: 1.5 h / 20 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.2: 6 h / 20 °C / Inert atmosphere

3.1: trimethylsilyl trifluoromethanesulfonate; triethylamine / dichloromethane / 8 h / Inert atmosphere; Reflux

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10 h / 0 - 20 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

6.1: Oxone; 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate / water; acetonitrile / 3 h / 8 - 10 °C

With Oxone; 1,1,1-trifluoro-2-propanone; trimethylsilyl trifluoromethanesulfonate; water; sodium hexamethyldisilazane; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; water; acetonitrile;
DOI:10.1039/c0cc05405d