4-{2-[(3-anthracen-9-yl-propyl)-methylamino]-ethoxy}-2-[1,3]dioxan-2-ylmethyl-phenylamine

Base Information

Chemical Name:4-{2-[(3-anthracen-9-yl-propyl)-methylamino]-ethoxy}-2-[1,3]dioxan-2-ylmethyl-phenylamine
CAS No.:705961-57-5
Molecular Formula:C₃₁H₃₆N₂O₃
Molecular Weight:484.638
Hs Code.:

Synonyms:4-{2-[(3-anthracen-9-yl-propyl)-methylamino]-ethoxy}-2-[1,3]dioxan-2-ylmethyl-phenylamine

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Chemical Property of 4-{2-[(3-anthracen-9-yl-propyl)-methylamino]-ethoxy}-2-[1,3]dioxan-2-ylmethyl-phenylamine

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Technology Process of 4-{2-[(3-anthracen-9-yl-propyl)-methylamino]-ethoxy}-2-[1,3]dioxan-2-ylmethyl-phenylamine

There total 9 articles about 4-{2-[(3-anthracen-9-yl-propyl)-methylamino]-ethoxy}-2-[1,3]dioxan-2-ylmethyl-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 705961-55-3
N-[2-(4-amino-3-[1,3]dioxan-2-ylmethyl-phenoxy)-ethyl]-3-anthracen-9-yl-N-methyl-propionamide

: 705961-57-5
4-{2-[(3-anthracen-9-yl-propyl)-methylamino]-ethoxy}-2-[1,3]dioxan-2-ylmethyl-phenylamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 16h;
DOI:10.1039/b400110a

Reference yield:

: 705961-44-0
3-[1,3]dioxan-2-ylmethyl-4-nitrophenol

: 705961-57-5
4-{2-[(3-anthracen-9-yl-propyl)-methylamino]-ethoxy}-2-[1,3]dioxan-2-ylmethyl-phenylamine

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / K₂CO₃ / dimethylformamide / 2 h / 90 °C

2: 98 percent / Amberlyst H-15 / tetrahydrofuran / 24 h / 20 °C

3: 89 percent / NaBH₄; iodine / tetrahydrofuran / 4 h / Heating

4: 93 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C

5: 89 percent / NaBH₄ / copper acetylacetonate / CH₂Cl₂; propan-2-ol; methanol / 0.5 h / Heating

6: 90 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 16 h / 20 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; Amberlyst H-15; iodine; potassium carbonate; triethylamine; copper acetylacetonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1039/b400110a

Reference yield:

: 2581-34-2,910311-23-8
3-methyl-4-nitrophenol

: 705961-57-5
4-{2-[(3-anthracen-9-yl-propyl)-methylamino]-ethoxy}-2-[1,3]dioxan-2-ylmethyl-phenylamine

Guidance literature:: Multi-step reaction with 10 steps

1.1: 91 percent / K₂CO₃ / dimethylformamide / 2 h / 90 °C

2.1: dimethylformamide / 24 h / Heating

2.2: 82 percent / aq. HCl / diethyl ether / 2 h / Heating

3.1: 93 percent / trifluoroacetic acid / 24 h / 20 °C

4.1: 92 percent / Amberlyst H-15 / CH₂Cl₂ / 16 h / 20 °C

5.1: 98 percent / K₂CO₃ / dimethylformamide / 2 h / 90 °C

6.1: 98 percent / Amberlyst H-15 / tetrahydrofuran / 24 h / 20 °C

7.1: 89 percent / NaBH₄; iodine / tetrahydrofuran / 4 h / Heating

8.1: 93 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C

9.1: 89 percent / NaBH₄ / copper acetylacetonate / CH₂Cl₂; propan-2-ol; methanol / 0.5 h / Heating

10.1: 90 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 16 h / 20 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; Amberlyst H-15; iodine; potassium carbonate; triethylamine; trifluoroacetic acid; copper acetylacetonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1039/b400110a