(S)-1-O-benzyl-2-O-<(diisopropylphosphono)methyl>-3-fluoro-1,2-propanediol

Base Information

Chemical Name:(S)-1-O-benzyl-2-O-<(diisopropylphosphono)methyl>-3-fluoro-1,2-propanediol
CAS No.:151223-08-4
Molecular Formula:C₁₇H₂₈FO₅P
Molecular Weight:362.378
Hs Code.:

Synonyms:(S)-1-O-benzyl-2-O-<(diisopropylphosphono)methyl>-3-fluoro-1,2-propanediol

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Chemical Property of (S)-1-O-benzyl-2-O-<(diisopropylphosphono)methyl>-3-fluoro-1,2-propanediol

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Technology Process of (S)-1-O-benzyl-2-O-<(diisopropylphosphono)methyl>-3-fluoro-1,2-propanediol

There total 3 articles about (S)-1-O-benzyl-2-O-<(diisopropylphosphono)methyl>-3-fluoro-1,2-propanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 941293-48-7
(S)-3-(benzyloxy)-2-[(diisopropoxyphosphoryl)methoxy]propyl 4-methylbenzenesulphonate

: 151223-08-4
(S)-1-O-benzyl-2-O-<(diisopropylphosphono)methyl>-3-fluoro-1,2-propanediol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; 1,4-dioxane; at 100 - 110 ℃; for 6.5h;
DOI:10.1016/j.tet.2019.130529

Reference yield: 77.0%

: 151223-06-2
(S)-3-O-benzyl-2-O-<(diisopropylphosphono)methyl>-1-O-(methylsulfonyl)glycerol

: 151223-08-4
(S)-1-O-benzyl-2-O-<(diisopropylphosphono)methyl>-3-fluoro-1,2-propanediol

Guidance literature:: With tri-n-butylamine hydrofluoride; In tetrahydrofuran; for 6h; Ambient temperature;
DOI:10.1021/jm00071a003

Reference yield: 50.0%

: 941293-70-5
diisopropyl (R)-((((1-benzyloxy)-3-hydroxypropan-2-yl)oxy)methyl)phosphonate

: 151223-08-4
(S)-1-O-benzyl-2-O-<(diisopropylphosphono)methyl>-3-fluoro-1,2-propanediol

Guidance literature:: With Nonafluorobutanesulfonyl fluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 90 ℃; for 4h;
DOI:10.1016/j.tet.2019.130529