N-(4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-yl)-2-methoxyacetamide

Base Information

Chemical Name:N-(4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-yl)-2-methoxyacetamide
CAS No.:1337932-07-6
Molecular Formula:C₁₅H₁₃Cl₂N₃O₅
Molecular Weight:386.191
Hs Code.:

Synonyms:N-(4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-yl)-2-methoxyacetamide

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Chemical Property of N-(4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-yl)-2-methoxyacetamide

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Technology Process of N-(4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-yl)-2-methoxyacetamide

There total 3 articles about N-(4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-yl)-2-methoxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 38870-89-2
Methoxyacetyl chloride

: 1337932-11-2
4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-amine

: 1337932-07-6
N-(4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-yl)-2-methoxyacetamide

Guidance literature:: Methoxyacetyl chloride; 4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-amine; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

With ammonia; In tetrahydrofuran; methanol; for 1h;

Reference yield:

: 105250-17-7
2-amino-4-hydroxymethylpyridine

: 1337932-07-6
N-(4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-yl)-2-methoxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.2: 1 h

With sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; mineral oil;

Reference yield:

: 36556-51-1
2,3-dichloro-1-fluoro-4-nitrobenzene

: 1337932-07-6
N-(4-((2,3-dichloro-4-nitrophenoxy)methyl)pyridin-2-yl)-2-methoxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.2: 1 h

With sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; mineral oil;