(1,1-difluoro-2-phenyl-ethyl)-phosphonodithioic acid S,S-diethyl ester

Base Information

Chemical Name:(1,1-difluoro-2-phenyl-ethyl)-phosphonodithioic acid S,S-diethyl ester
CAS No.:643013-49-4
Molecular Formula:C₁₂H₁₇F₂OPS₂
Molecular Weight:310.369
Hs Code.:

(1,1-difluoro-2-phenyl-ethyl)-phosphonodithioic acid <i>S</i>,<i>S</i>-diethyl ester

Synonyms:(1,1-difluoro-2-phenyl-ethyl)-phosphonodithioic acid S,S-diethyl ester

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Chemical Property of (1,1-difluoro-2-phenyl-ethyl)-phosphonodithioic acid S,S-diethyl ester

Chemical Property:

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Technology Process of (1,1-difluoro-2-phenyl-ethyl)-phosphonodithioic acid S,S-diethyl ester

There total 3 articles about (1,1-difluoro-2-phenyl-ethyl)-phosphonodithioic acid S,S-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-08-1
ethanethiol

: 643013-47-2
C₈H₇Cl₂F₂OP

: 643013-49-4
(1,1-difluoro-2-phenyl-ethyl)-phosphonodithioic acid S,S-diethyl ester

Guidance literature:: With triethylamine; In diethyl ether; at 20 ℃; for 16h;
DOI:10.1016/j.tetlet.2003.09.195

Reference yield:

: 100-39-0
benzyl bromide

: 643013-49-4
(1,1-difluoro-2-phenyl-ethyl)-phosphonodithioic acid S,S-diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / pyridine / 72 h / Heating

2: Et₃N / diethyl ether / 16 h / 20 °C

With thionyl chloride; triethylamine; In pyridine; diethyl ether;
DOI:10.1016/j.tetlet.2003.09.195

Reference yield:

: 126181-56-4
diethyl (1,1-difluoro-2-phenylethyl)phosphonate

: 643013-49-4
(1,1-difluoro-2-phenyl-ethyl)-phosphonodithioic acid S,S-diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / pyridine / 72 h / Heating

2: Et₃N / diethyl ether / 16 h / 20 °C

With thionyl chloride; triethylamine; In pyridine; diethyl ether;
DOI:10.1016/j.tetlet.2003.09.195