N-[2-{(cyclohexylideneamino)oxy}-2-methylpropyl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-[2-{(cyclohexylideneamino)oxy}-2-methylpropyl]-4-methylbenzenesulfonamide
CAS No.:1575701-71-1
Molecular Formula:C₁₇H₂₆N₂O₃S
Molecular Weight:338.471
Hs Code.:

Synonyms:N-[2-{(cyclohexylideneamino)oxy}-2-methylpropyl]-4-methylbenzenesulfonamide

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Chemical Property of N-[2-{(cyclohexylideneamino)oxy}-2-methylpropyl]-4-methylbenzenesulfonamide

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Technology Process of N-[2-{(cyclohexylideneamino)oxy}-2-methylpropyl]-4-methylbenzenesulfonamide

There total 4 articles about N-[2-{(cyclohexylideneamino)oxy}-2-methylpropyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 941-55-9
4-toluenesulfonyl azide

: 1575700-07-0
cyclohexanone O-(tert-butyl) oxime

: 1575701-71-1
N-[2-{(cyclohexylideneamino)oxy}-2-methylpropyl]-4-methylbenzenesulfonamide

: N,N'-[2-{(cyclohexylideneamino)oxy}-2-methylpropane-1,3-diyl]bis(4-methylbenzenesulfonamide)

Guidance literature:: With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; Ag⁽¹⁺⁾*C₂HF₆NO₄S₂; cesium acetate; In 1,2-dichloro-ethane; at 60 ℃; for 24h;
DOI:10.1039/c4cc05655h

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1575701-71-1
N-[2-{(cyclohexylideneamino)oxy}-2-methylpropyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 115 °C

2: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) triflimide; silver(I) acetate / 1,2-dichloro-ethane / 24 h / 25 - 60 °C

With pyridine; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) acetate; silver(I) triflimide; In 1,2-dichloro-ethane;
DOI:10.1021/ja501014b

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1575701-71-1
N-[2-{(cyclohexylideneamino)oxy}-2-methylpropyl]-4-methylbenzenesulfonamide

: N,N'-[2-{(cyclohexylideneamino)oxy}-2-methylpropane-1,3-diyl]bis(4-methylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / water; acetone / 11 h / 0 - 20 °C

2: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; Ag⁽¹⁺⁾*C₂HF₆NO₄S₂; cesium acetate / 1,2-dichloro-ethane / 24 h / 60 °C

With sodium azide; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; Ag⁽¹⁺⁾*C₂HF₆NO₄S₂; cesium acetate; In water; 1,2-dichloro-ethane; acetone;
DOI:10.1039/c4cc05655h