(+)-[2S-(2R,3R,4S,5S)6E]-8-allyloxy-5-methoxy-3-[(4-methoxyphenyl)methoxy]-2,4-dimethyl-6-octenal

Base Information

Chemical Name:(+)-[2S-(2R*,3R*,4S*,5S*)6E]-8-allyloxy-5-methoxy-3-[(4-methoxyphenyl)methoxy]-2,4-dimethyl-6-octenal
CAS No.:1253858-70-6
Molecular Formula:C₂₂H₃₂O₅
Molecular Weight:376.493
Hs Code.:

Synonyms:(+)-[2S-(2R*,3R*,4S*,5S*)6E]-8-allyloxy-5-methoxy-3-[(4-methoxyphenyl)methoxy]-2,4-dimethyl-6-octenal

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Chemical Property of (+)-[2S-(2R*,3R*,4S*,5S*)6E]-8-allyloxy-5-methoxy-3-[(4-methoxyphenyl)methoxy]-2,4-dimethyl-6-octenal

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Technology Process of (+)-[2S-(2R*,3R*,4S*,5S*)6E]-8-allyloxy-5-methoxy-3-[(4-methoxyphenyl)methoxy]-2,4-dimethyl-6-octenal

There total 1 articles about (+)-[2S-(2R*,3R*,4S*,5S*)6E]-8-allyloxy-5-methoxy-3-[(4-methoxyphenyl)methoxy]-2,4-dimethyl-6-octenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1253858-69-3
C₂₂H₃₄O₅

: 1253858-70-6
(+)-[2S-(2R*,3R*,4S*,5S*)6E]-8-allyloxy-5-methoxy-3-[(4-methoxyphenyl)methoxy]-2,4-dimethyl-6-octenal

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo101598y

Reference yield: 65.0%

: 75-77-4
chloro-trimethyl-silane

: 1253858-70-6
(+)-[2S-(2R*,3R*,4S*,5S*)6E]-8-allyloxy-5-methoxy-3-[(4-methoxyphenyl)methoxy]-2,4-dimethyl-6-octenal

: 130573-43-2
(2,2-dimethyl-6-methylene-6H-1,3-dioxin-4-yloxy)trimethylsilane

: 1253858-72-8
(-)-6-{[2S-(2R*,3R*,4R*,5S*,6S*)7E]-9-allyloxy-4-[(4-methoxyphenyl)methoxy]-6-methoxy-3,5-dimethyl-2-[(trimethylsilyl)oxy]non-7-enyl}-2,2-dimethyl-4H-1,3-dioxin-4-one

Guidance literature:: (+)-[2S-(2R*,3R*,4S*,5S*)6E]-8-allyloxy-5-methoxy-3-[(4-methoxyphenyl)methoxy]-2,4-dimethyl-6-octenal; (2,2-dimethyl-6-methylene-6H-1,3-dioxin-4-yloxy)trimethylsilane; With trifluoroborane diethyl ether; In dichloromethane; at -78 ℃; for 0.75h; Inert atmosphere;

chloro-trimethyl-silane; With triethylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo101598y