[(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co₂(diphenyl phosphato)2](ClO₄)*H₂O

Base Information

• Chemical Name: [(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co₂(diphenyl phosphato)2](ClO₄)*H₂O
• CAS No.: 1035457-06-7
• Molecular Formula: C₆₀H₅₉Co₂N₆O₉P₂*ClO₄*H₂O
• Molecular Weight: 1305.56

Synonyms:[(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co₂(diphenyl phosphato)2](ClO₄)*H₂O

Chemical Property of [(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co₂(diphenyl phosphato)2](ClO₄)*H₂O

Chemical Property:

Purity/Quality:

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Technology Process of [(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co₂(diphenyl phosphato)2](ClO₄)*H₂O

There total 1 articles about [(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co₂(diphenyl phosphato)2](ClO₄)*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

diphenyl hydrogen phosphate (838-85-7) + cobalt(II) perchlorate hexahydrate + 2,6?bis{[bis(2?pyridylmethyl)amino]methyl}?4?t?butylphenol (202128-99-2) → [(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co2(diphenyl phosphato)2](ClO4)*H2O (1035457-06-7)

Guidance literature:

In acetonitrile; HOC6H2(CH2N(CH2C5H4N)2)2C(CH3)3 and Co salt dissolved in MeCN, a soln. of HO2P(OC6H5)2 added; cooled, left in a refrigerator overnight, sepd., washed (cold MeCN); also the mother liquor concd., a soln. of NaOH added to give a second crop;recrystd. by slow evapn. of a MeCN soln. contg. NaClO4*H2O; elem. anal.;

DOI:10.1021/ic7020534

Reference yield: 70.0%

sodium perchlorate monohydrate (7791-07-3) + [(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co2(diphenyl phosphato)2](ClO4)*H2O (1035457-06-7) + acetone (67-64-1) → [(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co2(diphenyl phosphato)2](ClO4)2*(acetone)*H2O

Guidance literature:

With (NH₄)2[Ce(NO₃)6]; In N,N-dimethyl-formamide; Ce complex added to a soln. of Co complex, a soln. of Na salt added; pptd. (H2O), recrystd. (acetone/H2O); obtained as a mixt. of polymorphs;elem. anal.;

DOI:10.1021/ic7020534

Reference yield: 53.0%

sodium perchlorate monohydrate (7791-07-3) + [(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co2(diphenyl phosphato)2](ClO4)*H2O (1035457-06-7) + water (7732-18-5) → [(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co2(diphenyl phosphato)2](ClO4)3*3.5H2O

Guidance literature:

With (NH₄)2[Ce(NO₃)6]; In N,N-dimethyl-formamide; Ce complex added to a soln. of Co complex, a soln. of Na salt added; pptd. (H2O), recrystd. (acetone/H2O); elem. anal.;

DOI:10.1021/ic7020534

upstream raw materials:

diphenyl hydrogen phosphate

2,6?bis{[bis(2?pyridylmethyl)amino]methyl}?4?t?butylphenol

Downstream raw materials:

[(2,6-bis((N,N'-bis-(2-pyridylmethyl)amino)methyl)-4-tertbutylphenolato)Co₂(diphenyl phosphato)2](B(Ph)4)

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