Technology Process of 1-methoxy-6-pentylcyclohexa-1,4-diene
There total 1 articles about 1-methoxy-6-pentylcyclohexa-1,4-diene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonia; potassium; iron(III) chloride;
for 0.166667h;
Yield given;
DOI:10.1039/P19830000007
- Guidance literature:
-
Multi-step reaction with 6 steps
1: aq. 10percent H2SO4 / methanol; H2O / 1 h / Ambient temperature
2: 90 percent / hydrogen peroxide, potassium hydroxide / methanol; H2O / 1 h / 15 °C
3: 7.8 g / tosyl hydrazine / acetic acid; CH2Cl2 / 8 h / Ambient temperature
4: 2.2 g / tetrahydrofuran / 3 h / Ambient temperature
5: 1.62 g / pyridine-chromic anhydride complex / CH2Cl2 / 0.25 h / Ambient temperature
6: 1.6 g / hydrogen, pyridine / 10percent Pd-BaSO4 / ethyl acetate
With
pyridine; potassium hydroxide; pyridinium dichromate; sulfuric acid; hydrogen; dihydrogen peroxide; toluene-4-sulfonic acid hydrazide;
palladium on barium sulfate;
In
tetrahydrofuran; methanol; dichloromethane; water; acetic acid; ethyl acetate;
DOI:10.1039/P19830000007
- Guidance literature:
-
With
sulfuric acid;
In
methanol; water;
for 1h;
Yield given;
Ambient temperature;
DOI:10.1039/P19830000007