5-(tert-butyl)-2-hydroxy-3-(6-(trifluoromethyl)pyridin-3-yl)benzaldehyde oxime

Base Information

Chemical Name:5-(tert-butyl)-2-hydroxy-3-(6-(trifluoromethyl)pyridin-3-yl)benzaldehyde oxime
CAS No.:1609654-84-3
Molecular Formula:C₁₇H₁₇F₃N₂O₂
Molecular Weight:338.329
Hs Code.:

Synonyms:5-(tert-butyl)-2-hydroxy-3-(6-(trifluoromethyl)pyridin-3-yl)benzaldehyde oxime

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Chemical Property of 5-(tert-butyl)-2-hydroxy-3-(6-(trifluoromethyl)pyridin-3-yl)benzaldehyde oxime

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Technology Process of 5-(tert-butyl)-2-hydroxy-3-(6-(trifluoromethyl)pyridin-3-yl)benzaldehyde oxime

There total 4 articles about 5-(tert-butyl)-2-hydroxy-3-(6-(trifluoromethyl)pyridin-3-yl)benzaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1609654-73-0
5-(tert-butyl)-2-hydroxy-3-(6-(trifluoromethyl)pyridin-3-yl)benzaldehyde

: 1609654-84-3
5-(tert-butyl)-2-hydroxy-3-(6-(trifluoromethyl)pyridin-3-yl)benzaldehyde oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; at 20 ℃; for 16h;

Reference yield:

: 98-54-4
para-tert-butylphenol

: 1609654-84-3
5-(tert-butyl)-2-hydroxy-3-(6-(trifluoromethyl)pyridin-3-yl)benzaldehyde oxime

Guidance literature:: Multi-step reaction with 4 steps

1.1: bromine / chloroform; tetrachloromethane / 0 °C / Inert atmosphere

2.1: trifluoroacetic acid / 22 h / 90 °C / Inert atmosphere

3.1: potassium carbonate / 1,2-dimethoxyethane; water / 0.33 h / Inert atmosphere

3.2: 24 h / 80 °C / Inert atmosphere; Sealed tube

4.1: sodium acetate; hydroxylamine hydrochloride / ethanol / 16 h / 20 °C

With hydroxylamine hydrochloride; bromine; sodium acetate; potassium carbonate; trifluoroacetic acid; In tetrachloromethane; 1,2-dimethoxyethane; ethanol; chloroform; water; 2.1: |Duff Aldehyde Synthesis / 3.1: |Suzuki Coupling / 3.2: |Suzuki Coupling;

Reference yield:

: 2198-66-5
2-bromo-4-tert-butylphenol

: 1609654-84-3
5-(tert-butyl)-2-hydroxy-3-(6-(trifluoromethyl)pyridin-3-yl)benzaldehyde oxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / 22 h / 90 °C / Inert atmosphere

2.1: potassium carbonate / 1,2-dimethoxyethane; water / 0.33 h / Inert atmosphere

2.2: 24 h / 80 °C / Inert atmosphere; Sealed tube

3.1: sodium acetate; hydroxylamine hydrochloride / ethanol / 16 h / 20 °C

With hydroxylamine hydrochloride; sodium acetate; potassium carbonate; trifluoroacetic acid; In 1,2-dimethoxyethane; ethanol; water; 1.1: |Duff Aldehyde Synthesis / 2.1: |Suzuki Coupling / 2.2: |Suzuki Coupling;