norbornane-2-carbaldehyde

Base Information

Chemical Name:norbornane-2-carbaldehyde
CAS No.:3574-54-7
Molecular Formula:C8H12O
Molecular Weight:124.183
Hs Code.:
Mol file:3574-54-7.mol

Synonyms:

Suppliers and Price of norbornane-2-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 5 raw suppliers

Chemical Property of norbornane-2-carbaldehyde

Chemical Property:

Boiling Point:182.5°Cat760mmHg
Flash Point:58.1°C
Density:1.11g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of norbornane-2-carbaldehyde

There total 6 articles about norbornane-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 86553-92-6
Bicyclo<2.2.1>heptan-1-oxiran-2-ylmethyltrimethylsilane

: 3574-54-7,3574-55-8,19396-83-9,69769-91-1,69769-92-2,104418-69-1,110849-52-0,135818-35-8
3-formyl-bicyclo<2.2.1>heptane

Guidance literature:: With tetrahydrofuran; perchloric acid; at 20 ℃; for 10h;
DOI:10.1016/S0040-4020(01)88585-9

Reference yield:

: 120-74-1,934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7
5-carboxybicyclo<2.2.1>hept-2-ene

: 3574-54-7
2-endo-Bicyclo<2.2.1>heptanecarboxaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / 1,2-dichloro-ethane / 2 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 40 °C

3.1: hydrogen; palladium 10% on activated carbon / ethyl acetate / 4.17 h / 20 °C

4.1: oxalyl dichloride / dimethyl sulfoxide; dichloromethane / 0.5 h / -75 - -70 °C

4.2: 0.33 h / -75 - -68 °C

With dmap; lithium aluminium tetrahydride; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1021/acs.jmedchem.0c00359

Reference yield:

: 201230-82-2
carbon monoxide

: 498-66-8
norbornene

: 3574-54-7,3574-55-8,19396-83-9,69769-91-1,69769-92-2,104418-69-1,110849-52-0,135818-35-8
3-formyl-bicyclo<2.2.1>heptane

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; (acetylacetonato)dicarbonylrhodium (l); hydrogen; In tert-butyl alcohol; at 35 ℃; for 20h; under 2327.23 Torr; Inert atmosphere; Large scale reaction;
DOI:10.1021/op100284a