C₁₇H₂₄N₂O

Base Information

Chemical Name:C₁₇H₂₄N₂O
CAS No.:1255097-46-1
Molecular Formula:C₁₇H₂₄N₂O
Molecular Weight:272.39
Hs Code.:

C<sub>17</sub>H<sub>24</sub>N<sub>2</sub>O

Synonyms:C₁₇H₂₄N₂O

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Chemical Property of C₁₇H₂₄N₂O

Chemical Property:

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Technology Process of C₁₇H₂₄N₂O

There total 6 articles about C₁₇H₂₄N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1255097-44-9
C₁₀H₁₈N₂O

: 100-39-0
benzyl bromide

: 1255097-46-1
C₁₇H₂₄N₂O

Guidance literature:: C₁₀H₁₈N₂O; With n-butyllithium; In tetrahydrofuran; at 0 ℃;

With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -50 ℃;

benzyl bromide; In tetrahydrofuran; at -50 ℃;
DOI:10.1246/cl.2010.835

Reference yield:

: 562-13-0
2,2-dimethyl-1,3-cyclohexanedione

: 1255097-46-1
C₁₇H₂₄N₂O

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 - 0 °C

2.1: (-)-diisopinocamphenylborane chloride / 24 h / 20 °C

3.1: N-iodo-succinimide / dichloromethane / 2 h / -40 - 20 °C

4.1: 2,6-dimethylpyridine; silver trifluoromethanesulfonate / dichloromethane / 2 h / 40 °C

5.1: acetic acid / ethanol / 12 h / 70 °C

6.1: n-butyllithium / tetrahydrofuran / 0 °C

6.2: -50 °C

6.3: -50 °C

With 2,6-dimethylpyridine; N-iodo-succinimide; n-butyllithium; silver trifluoromethanesulfonate; potassium hexamethylsilazane; acetic acid; (-)-diisopinocamphenylborane chloride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1246/cl.2010.835

Reference yield:

: 1255097-40-5
C₁₇H₃₂O₂Si

: 1255097-46-1
C₁₇H₂₄N₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: (-)-diisopinocamphenylborane chloride / 24 h / 20 °C

2.1: N-iodo-succinimide / dichloromethane / 2 h / -40 - 20 °C

3.1: 2,6-dimethylpyridine; silver trifluoromethanesulfonate / dichloromethane / 2 h / 40 °C

4.1: acetic acid / ethanol / 12 h / 70 °C

5.1: n-butyllithium / tetrahydrofuran / 0 °C

5.2: -50 °C

5.3: -50 °C

With 2,6-dimethylpyridine; N-iodo-succinimide; n-butyllithium; silver trifluoromethanesulfonate; acetic acid; (-)-diisopinocamphenylborane chloride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1246/cl.2010.835