4,9-dioxo-3-methyl-1-(3,4,5-trimethoxyphenyl)naphtho[2,3-d][1,2,3]triazol-3-ium trifluoromethanesulfonate

Base Information

Chemical Name:4,9-dioxo-3-methyl-1-(3,4,5-trimethoxyphenyl)naphtho[2,3-d][1,2,3]triazol-3-ium trifluoromethanesulfonate
CAS No.:1600529-75-6
Molecular Formula:CF₃O₃S*C₂₀H₁₈N₃O₅
Molecular Weight:529.45
Hs Code.:

Synonyms:4,9-dioxo-3-methyl-1-(3,4,5-trimethoxyphenyl)naphtho[2,3-d][1,2,3]triazol-3-ium trifluoromethanesulfonate

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Chemical Property of 4,9-dioxo-3-methyl-1-(3,4,5-trimethoxyphenyl)naphtho[2,3-d][1,2,3]triazol-3-ium trifluoromethanesulfonate

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Technology Process of 4,9-dioxo-3-methyl-1-(3,4,5-trimethoxyphenyl)naphtho[2,3-d][1,2,3]triazol-3-ium trifluoromethanesulfonate

There total 3 articles about 4,9-dioxo-3-methyl-1-(3,4,5-trimethoxyphenyl)naphtho[2,3-d][1,2,3]triazol-3-ium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1600529-59-6
1-(3,4,5-trimethoxyphenyl)-1H-naphtho[2,3-d][1,2,3]triazole-4,9-dione

: 333-27-7
methyl trifluoromethanesulfonate

: 1600529-75-6
4,9-dioxo-3-methyl-1-(3,4,5-trimethoxyphenyl)naphtho[2,3-d][1,2,3]triazol-3-ium trifluoromethanesulfonate

Guidance literature:: In toluene; at 100 ℃;
DOI:10.1016/j.ejmech.2014.02.060

Reference yield:

: 24313-88-0
3,4,5-Trimethoxyaniline

: 1600529-75-6
4,9-dioxo-3-methyl-1-(3,4,5-trimethoxyphenyl)naphtho[2,3-d][1,2,3]triazol-3-ium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.17 h / 0 °C

1.2: 1.5 h / 20 °C

2.1: N,N-dimethyl-formamide / 48 h / 60 °C

3.1: toluene / 100 °C

With hydrogenchloride; sodium nitrite; In water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.ejmech.2014.02.060

Reference yield:

: 115483-29-9
3,4,5-trimethoxyphenyl azide

: 1600529-75-6
4,9-dioxo-3-methyl-1-(3,4,5-trimethoxyphenyl)naphtho[2,3-d][1,2,3]triazol-3-ium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 48 h / 60 °C

2: toluene / 100 °C

In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.ejmech.2014.02.060