2-fluoro-5-iodobenzoyl chloride oxime

Base Information

• Chemical Name: 2-fluoro-5-iodobenzoyl chloride oxime
• CAS No.: 334971-56-1
• Molecular Formula: C₇H₄ClFINO
• Molecular Weight: 299.471
• Mol file: 334971-56-1.mol

Synonyms:2-fluoro-5-iodobenzoyl chloride oxime

Chemical Property of 2-fluoro-5-iodobenzoyl chloride oxime

Chemical Property:

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Technology Process of 2-fluoro-5-iodobenzoyl chloride oxime

There total 1 articles about 2-fluoro-5-iodobenzoyl chloride oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-fluoro-5-iodobenzaldehyde oxime (334971-55-0) → 2-fluoro-5-iodobenzoyl chloride oxime (334971-56-1)

Guidance literature:

With hydrogenchloride; N-chloro-succinimide; In DMF (N,N-dimethyl-formamide); at 25 - 40 ℃; for 2h;

Reference yield: 73.0%

2-fluoro-5-iodobenzoyl chloride oxime (334971-56-1) + Ethyl 2-butynoate (4341-76-8) → 4-ethoxycarbonyl-5-methyl-3-(2-fluoro-5-iodophenyl)isoxazole (334971-57-2)

Guidance literature:

With triethylamine; In diethyl ether; at 0 - 20 ℃; for 1h; Nitrogen gasification;

upstream raw materials:

2-fluoro-5-iodobenzaldehyde oxime

Downstream raw materials:

4-ethoxycarbonyl-5-methyl-3-(2-fluoro-5-iodophenyl)isoxazole