(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

Base Information

Chemical Name:(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside
CAS No.:155739-81-4
Molecular Formula:C₃₂H₄₁NO₁₅
Molecular Weight:679.675
Hs Code.:

Synonyms:(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

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Technology Process of (2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

There total 10 articles about (2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 92841-84-4
allyl 2-acetamido-2-deoxy-4,6-O-benzylidene-α-D-galactopyranoside

: 3068-32-4
1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

: 155739-81-4
(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

Guidance literature:: With mercury(II) cyanide; In nitromethane; benzene; at 20 ℃; for 18h;
DOI:10.1021/ja002596w

Reference yield: 78.0%

: 174851-20-8
allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranose

: 3068-32-4
1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

: 155739-81-4
(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

Guidance literature:: With mercury(II) cyanide; In nitromethane; benzene; at 25 ℃;
DOI:10.1039/b008664i

Reference yield:

: 64650-83-5
N-((2S,3R,4R,5R,6R)-2-Allyloxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-acetamide

: 155739-81-4
(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / ZnCl₂ / 25 °C

2: 78 percent / nitromethane; benzene / 25 °C

With zinc(II) chloride; In nitromethane; benzene;
DOI:10.1016/S0968-0896(01)00248-6