benzoylimino-fluoren-9-yl-sulfonium betaine

Base Information

• Chemical Name: benzoylimino-fluoren-9-yl-sulfonium betaine
• CAS No.: 39593-85-6
• Molecular Formula: C₂₀H₁₃NOS
• Molecular Weight: 315.395
• Mol file: 39593-85-6.mol

Synonyms:benzoylimino-fluoren-9-yl-sulfonium betaine

Chemical Property of benzoylimino-fluoren-9-yl-sulfonium betaine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzoylimino-fluoren-9-yl-sulfonium betaine

There total 5 articles about benzoylimino-fluoren-9-yl-sulfonium betaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzoyl-S-(9-chloro-fluoren-9-yl)-thiohydroxylamine (39593-83-4) → benzoylimino-fluoren-9-yl-sulfonium betaine (39593-85-6)

Guidance literature:

With triethylamine; In tetrahydrofuran;

DOI:10.1021/jo00933a014

Reference yield:

N-trimethylsilylbenzamide (1011-57-0) → benzoylimino-fluoren-9-yl-sulfonium betaine (39593-85-6)

Guidance literature:

Multi-step reaction with 3 steps

1: SCl₂

3: Et₃N / tetrahydrofuran

With sulfur dichloride; triethylamine; In tetrahydrofuran;

DOI:10.1021/jo00933a014

Reference yield:

N-benzoyl-S-chloro-thiohydroxylamine (39593-81-2) → benzoylimino-fluoren-9-yl-sulfonium betaine (39593-85-6)

Guidance literature:

Multi-step reaction with 2 steps

2: Et₃N / tetrahydrofuran

With triethylamine; In tetrahydrofuran;

DOI:10.1021/jo00933a014

upstream raw materials:

N-benzoyl-S-(9-chloro-fluoren-9-yl)-thiohydroxylamine

N-trimethylsilylbenzamide

N-benzoyl-S-chloro-thiohydroxylamine

benzamide

Downstream raw materials:

6-diethylamino-4-fluoren-9-yl-5-methyl-2-phenyl-[1,4,3]oxathiazinium betaine

2'-benzoyl-4't-methyl-3'r-piperidin-1-yl-spiro[fluorene-9,5'-isothiazolidine] 1'ξ-oxide

2'-benzoyl-4',4'-dimethyl-3'-pyrrolidin-1-yl-spiro[fluorene-9,5'-isothiazolidine] 1'-oxide

2'-benzoyl-4't-methyl-3'r-piperidin-1-yl-spiro[fluorene-9,5'-isothiazolidine]